1,3-Dioxolan-4-one, 5-phenyl-, (S)-

Base Information

Chemical Name:1,3-Dioxolan-4-one, 5-phenyl-, (S)-
CAS No.:60646-33-5
Molecular Formula:C9H8O3
Molecular Weight:164.161
Hs Code.:
DSSTox Substance ID:DTXSID10473448
Nikkaji Number:J1.457.282A
Wikidata:Q82302848

Synonyms:1,3-Dioxolan-4-one, 5-phenyl-, (S)-;60646-33-5;DTXSID10473448

Suppliers and Price of 1,3-Dioxolan-4-one, 5-phenyl-, (S)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1,3-Dioxolan-4-one, 5-phenyl-, (S)-

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:164.047344113
Heavy Atom Count:12
Complexity:173

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1OC(C(=O)O1)C2=CC=CC=C2
Isomeric SMILES:C1O[C@H](C(=O)O1)C2=CC=CC=C2

Technology Process of 1,3-Dioxolan-4-one, 5-phenyl-, (S)-

There total 1 articles about 1,3-Dioxolan-4-one, 5-phenyl-, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 17199-29-0
(S)-Mandelic acid

: 60646-33-5
(5S)-5-phenyl-1,3-dioxolan-4-one

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 1h; Heating;
DOI:10.1016/S0040-4039(00)02104-3

Reference yield: 96.0%

: 60646-33-5
(5S)-5-phenyl-1,3-dioxolan-4-one

: 1099-45-2
ethyl (triphenylphosphoranylidene)acetate

: 333459-74-8
[(S)-5-Phenyl-[1,3]dioxolan-(4E)-ylidene]-acetic acid ethyl ester

Guidance literature:: In toluene; for 2h; Heating;
DOI:10.1016/S0040-4039(00)02104-3

Reference yield:

: 60646-33-5
(5S)-5-phenyl-1,3-dioxolan-4-one

: 145285-60-5
(4S,5S)-4-hydroxy-5-phenyldihydrofuran-2(3H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / toluene / 2 h / Heating

2: conc. HCl / ethanol / 4 h / Heating

3: NaBH₄ / methanol / 1 h / 0 °C

With hydrogenchloride; sodium tetrahydroborate; In methanol; ethanol; toluene; 1: Wittlg reaction;
DOI:10.1016/S0040-4039(00)02104-3