dichlorobis(ethylenediamine)iridium chloride

Base Information

• Chemical Name: dichlorobis(ethylenediamine)iridium chloride
• CAS No.: 15444-46-9
• Molecular Formula: C₄H₁₆Cl₃IrN₄
• Molecular Weight: 418.777
• Mol file: 15444-46-9.mol

Synonyms:Iridium(1+),dichlorobis(1,2-ethanediamine-N,N')-, chloride, (OC-6-12)-; Iridium(1+),dichlorobis(ethylenediamine)-, chloride, trans- (8CI);trans-Dichlorobis(ethylendiamine)iridium(1+) chloride;trans-Dichlorobis(ethylenediamine)iridium(1+) monochloride

Chemical Property of dichlorobis(ethylenediamine)iridium chloride

Chemical Property:

• PSA: 104.08000
• LogP: -4.00420

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of dichlorobis(ethylenediamine)iridium chloride

There total 2 articles about dichlorobis(ethylenediamine)iridium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

mer-trichloro(1,2-ethanediamine)-(2-aminoethylammonium)iridium(III) chloride hydrate → mer-trichloro(1,2-ethanediamine)-(2-aminoethylamine)iridium(III) (126783-11-7,15444-46-9,15444-47-0)

Guidance literature:

With KOH; In water; addn. of soln. Ir complex to soln. KOH; recrystn. (room temp., 2 h);

Reference yield: 39.0%

IrCl3*6.6H2O + ethylenediamine (107-15-3,85404-18-8) → cis-{Ir(en)2Cl2}Cl*H2O + trans-{Ir(en)2Cl2}Cl*H2O (126783-11-7,15444-46-9,15444-47-0)

Guidance literature:

With hydrogenchloride; acetic acid; In water; reflux for 5 h, then evapd. to dryness, the solid residue was heated to 170°C for 24 h, redissolved in boiling water, pptn. of cis-compound on standing, standing, washed with water; combined filtrate and washings heated, 12 M HCl was added and the mixture was allowed to stand at room temp. for 1 h then cooled in ice for 2 h, crystals of trans-compound washed with cold HCl, then with ethanol, dried at 135 °C; elem. anal.;

upstream raw materials:

ethylenediamine

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