5-(3-Methoxyphenyl)-3,3-dimethylcyclohexan-1-one

Base Information

Chemical Name:5-(3-Methoxyphenyl)-3,3-dimethylcyclohexan-1-one
CAS No.:60741-74-4
Molecular Formula:C₁₅H₂₀O₂
Molecular Weight:232.323
Hs Code.:
DSSTox Substance ID:DTXSID40519666

Synonyms:5-(3-Methoxyphenyl)-3,3-dimethylcyclohexan-1-one;60741-74-4;DTXSID40519666

Suppliers and Price of 5-(3-Methoxyphenyl)-3,3-dimethylcyclohexan-1-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(3-Methoxyphenyl)-3,3-dimethylcyclohexan-1-one

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:232.146329876
Heavy Atom Count:17
Complexity:283

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1(CC(CC(=O)C1)C2=CC(=CC=C2)OC)C

Technology Process of 5-(3-Methoxyphenyl)-3,3-dimethylcyclohexan-1-one

There total 1 articles about 5-(3-Methoxyphenyl)-3,3-dimethylcyclohexan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 4694-17-1
5,5-dimethlycyclohex-2-en-1-one

: 36282-40-3
(3-methoxyphenyl)magnesium bromide

: 60741-74-4
5-(3-Methoxy-phenyl)-3,3-dimethyl-cyclohexanone

Guidance literature:: With copper(l) chloride; In diethyl ether; -40 deg C, then rt.;
DOI:10.1248/cpb.31.3915

Reference yield:

: 60741-74-4
5-(3-Methoxy-phenyl)-3,3-dimethyl-cyclohexanone

: 64970-39-4,89674-21-5,89674-23-7
1,2-cis-2-dimethylaminomethyl-3-(3-methoxyphenyl)-5,5-dimethylcyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 10.5 g / ethanol / 10 h / 70 - 80 °C

2: 14 percent / LiAlH₄ / diethyl ether / 3 h / Heating

With lithium aluminium tetrahydride; In diethyl ether; ethanol;
DOI:10.1248/cpb.31.3915

Reference yield:

: 60741-74-4
5-(3-Methoxy-phenyl)-3,3-dimethyl-cyclohexanone

: 64970-39-4,89674-21-5,89674-23-7
1,2-trans-2-dimethylaminomethyl-3-(3-methoxyphenyl)-5,5-dimethylcyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 10.5 g / ethanol / 10 h / 70 - 80 °C

2: 59 percent / LiAlH₄ / diethyl ether / 3 h / Heating

With lithium aluminium tetrahydride; In diethyl ether; ethanol;
DOI:10.1248/cpb.31.3915