N-(9-anthracenylmethylene)-P-toluidine

Base Information

Chemical Name:N-(9-anthracenylmethylene)-P-toluidine
CAS No.:6076-00-2
Molecular Formula:C22H17N
Molecular Weight:295.384
Hs Code.:
European Community (EC) Number:666-748-0
ChEMBL ID:CHEMBL1927794
DSSTox Substance ID:DTXSID30401081

Synonyms:N-(9-anthracenylmethylene)-P-toluidine;6076-00-2;BIDD:GT0661;CHEMBL1927794;DTXSID30401081;AKOS003409626;(E)-1-(Anthracen-9-yl)-N-(4-methylphenyl)methanimine

Suppliers and Price of N-(9-anthracenylmethylene)-P-toluidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N-(9-anthracenylmethylene)-P-toluidine

Chemical Property:

XLogP3:6.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:295.136099547
Heavy Atom Count:23
Complexity:384

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)N=CC2=C3C=CC=CC3=CC4=CC=CC=C42

Technology Process of N-(9-anthracenylmethylene)-P-toluidine

There total 2 articles about N-(9-anthracenylmethylene)-P-toluidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 106-49-0,12221-03-3
p-toluidine

: 642-31-9
9-anthracene aldehyde

: 6076-00-2
4-methyl-N-(anthracene-9-ylmethylene)aniline

Guidance literature:: In methanol; at 120 ℃; Microwave irradiation; Sealed vessel; Inert atmosphere;
DOI:10.1016/j.jorganchem.2009.09.030

Reference yield:

: 1338600-14-8
[N-methyl(diethoxyphosphonyl)-1-(9-anthryl)]p-toluidine

: 6076-00-2
4-methyl-N-(anthracene-9-ylmethylene)aniline

Guidance literature:: With sodium hydroxide; In ethanol; Reflux;
DOI:10.1080/10426507.2011.638349

Reference yield: 82.0%

: 6076-00-2
4-methyl-N-(anthracene-9-ylmethylene)aniline

: 1600-27-7
mercury(II) diacetate

: HgCl(4-methyl-N-(anthracene-9-ylmethylene)aniline)

Guidance literature:: With LiCl; In methanol; under N2; Schiff base and Hg acetate stirred (24 h) together in refluxing MeOH, mixt. cooled, LiCl in hot MeOH added under stirring; ppt. filtered, washed (Et2O), dried, solid extd. by hexane via G-4 soxlet frit, recrystn. (CHCl3-MeOH, 1:1);
DOI:10.1016/j.jorganchem.2009.09.030