Benzenemethanol, a-methyl-a-phenyl-, 4-nitrobenzoate

Base Information

• Chemical Name: Benzenemethanol, a-methyl-a-phenyl-, 4-nitrobenzoate
• CAS No.: 60921-50-8
• Molecular Formula: C21H17NO4
• Molecular Weight: 347.37
• Mol file: 60921-50-8.mol

Synonyms:

Chemical Property of Benzenemethanol, a-methyl-a-phenyl-, 4-nitrobenzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenemethanol, a-methyl-a-phenyl-, 4-nitrobenzoate

There total 2 articles about Benzenemethanol, a-methyl-a-phenyl-, 4-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1-diphenylethanol (599-67-7) + 4-nitro-benzoyl chloride (122-04-3) → 1,1-diphenylethyl p-nitrobenzoate (60921-50-8)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; hexane; at -30 - 20 ℃;

DOI:10.1246/bcsj.75.1371

Reference yield:

→ 1,1-diphenylethyl p-nitrobenzoate (60921-50-8)

Guidance literature:

entspr. tert-Alkohol, n-Butyllithium, p-Nitrobenzoylchlorid;

DOI:10.1021/jo00426a031

Reference yield:

1,1-diphenylethyl p-nitrobenzoate (60921-50-8) → 1,1-Diphenylethylene (530-48-3)

Guidance literature:

With water; In acetone; at 25 ℃; Kinetics;

DOI:10.1002/poc.484

upstream raw materials:

1,1-diphenylethanol

4-nitro-benzoyl chloride

Downstream raw materials:

1,1-Diphenylethylene

Refernces