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4-Nitrobenzoyl chloride
Cas No: 122-04-3
No Data 1 Gram 50 Metric Ton/Month Hangzhou Zhongqi chem Co.,Ltd. Contact Supplier
4-Nitrobenzoyl chloride
Cas No: 122-04-3
No Data No Data No Data Aecochem Corp. Contact Supplier
4-Nitrobenzoyl chloride suppliers in China
Cas No: 122-04-3
No Data 100 Gram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
High quality P-Nitrobenzoyl Chloride supplier in China
Cas No: 122-04-3
No Data 1 Kilogram 2000 Metric Ton/Year Simagchem Corporation Contact Supplier
High purity 122-04-3 4-Nitrobenzoyl chloride
Cas No: 122-04-3
USD $ 100.0-500.0 / Gram 1 Gram 99999 Gram/Year Hangzhou Dingyan Chem Co., Ltd Contact Supplier
Factory Supply P-Nitrobenzoyl Chloride
Cas No: 122-04-3
No Data 1 1 Ality Chemical Corporation Contact Supplier
4-nitrobenzoyl chloride
Cas No: 122-04-3
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
4-Nitrobenzoyl chloride
Cas No: 122-04-3
No Data No Data No Data Shanghai Sunwise Chemical Co., Ltd Contact Supplier
4-Nitrobenzoyl chloride Factory stock High quality 4-Nitrobenzoyl chloride with best price CAS: 122-04-3
Cas No: 122-04-3
USD $ 1.0-2.0 / Metric Ton 5 Metric Ton 1000 Metric Ton/Year Henan Sinotech Import&Export Corporation Contact Supplier
High Purity 99% Pharmaceutical Intermediates 4-Nitrobenzoyl chloride
Cas No: 122-04-3
USD $ 3.0-3.0 / Gram 1 Gram 10 Metric Ton/Month Hebei yanxi chemical co.,LTD. Contact Supplier

122-04-3 Usage

Chemical Properties

yellow needles or powder

Uses

4-Nitrobenzoyl Chloride is used inorganic syntheses such as Michael additions. Also used in the synthesis of polysubstituted furanonaphthoquinoines.

Uses

4-Nitrobenzoyl chloride is used in the preparation of polysubstituted furanonaphthoquinoines. It is also involved in Michael addition, Henry reaction, O-alkylation and cycloaddition reactions. Further, it is employed as an intermediate in active pharmaceutical ingredient and dyes.

General Description

Yellow needles or powder with a pungent odor.

Air & Water Reactions

Unstable in moist surroundings and should be kept in a tightly-closed container. React with water or steam .

Reactivity Profile

4-Nitrobenzoyl chloride is incompatible with bases (including amines), with strong oxidizing agents, and with alcohols. May react with reducing agents. May react vigorously or explosively if mixed with diisopropyl ether or other ethers in the presence of trace amounts of metal salts [J. Haz. Mat., 1981, 4, 291].

Health Hazard

TOXIC; inhalation, ingestion or skin contact with material may cause severe injury or death. Contact with molten substance may cause severe burns to skin and eyes. Avoid any skin contact. Effects of contact or inhalation may be delayed. Fire may produce irritating, corrosive and/or toxic gases. Runoff from fire control or dilution water may be corrosive and/or toxic and cause pollution.

Fire Hazard

Flash point data are not available for 4-Nitrobenzoyl chloride, but 4-Nitrobenzoyl chloride is combustible.

Safety Profile

Moderately toxic by ingestion. Experimental reproductive effects. Mutation data reported. When heated to decomposition it emits toxic fumes of NOx and Cl-. See also NITRO COhlPOUNDS OF AROMATIC HYDROCARBONS and CHLORIDES.

Purification Methods

Crystallise the acid chloride from dry pet ether (b 60-80o), *C6H6 or CCl4. Distil it under vacuum. Irritant. [Adama & Jenkins Org Synth Coll Vol I 394 1941, Beilstein 9 III 1709, 9 IV 1191.]
InChI:InChI=1/C7H4ClNO3/c8-7(10)5-1-3-6(4-2-5)9(11)12/h1-4H

122-04-3 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (A12543)  4-Nitrobenzoyl chloride, 98%    122-04-3 10g 217.0CNY Detail
Alfa Aesar (A12543)  4-Nitrobenzoyl chloride, 98%    122-04-3 250g 443.0CNY Detail
Alfa Aesar (A12543)  4-Nitrobenzoyl chloride, 98%    122-04-3 1000g 1181.0CNY Detail
Sigma-Aldrich (73120)  4-Nitrobenzoylchloride  for HPLC derivatization, ≥99.0% (GC) 122-04-3 73120-25G 374.40CNY Detail
Sigma-Aldrich (73120)  4-Nitrobenzoylchloride  for HPLC derivatization, ≥99.0% (GC) 122-04-3 73120-100G 1,029.60CNY Detail
Sigma-Aldrich (73120)  4-Nitrobenzoylchloride  for HPLC derivatization, ≥99.0% (GC) 122-04-3 73120-500G 4,264.65CNY Detail
Aldrich (112208)  4-Nitrobenzoylchloride  98% 122-04-3 112208-50G 468.00CNY Detail
Aldrich (112208)  4-Nitrobenzoylchloride  98% 122-04-3 112208-250G 905.58CNY Detail
Aldrich (112208)  4-Nitrobenzoylchloride  98% 122-04-3 112208-500G 1,466.01CNY Detail

122-04-3SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name 4-Nitrobenzoyl chloride

1.2 Other means of identification

Product number -
Other names p-NO2-PhCO3tBu

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:122-04-3 SDS

122-04-3Synthetic route

(4-nitrophenyl)ethanone
100-19-6

(4-nitrophenyl)ethanone

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
Stage #1: (4-nitrophenyl)ethanone With pyridine; disulfur dichloride In chlorobenzene at 20℃; for 2.5h;
Stage #2: With sulfuryl dichloride In chlorobenzene at 20 - 132℃; for 21h; Reagent/catalyst; Temperature;
90%
Stage #1: (4-nitrophenyl)ethanone With pyridine; sulfur monochloride In chlorobenzene at 20℃;
Stage #2: With thionyl chloride In chlorobenzene at 20 - 132℃;
71%
With pyridine; disulfur dichloride at 70 - 138℃; for 21.5h;83 %Spectr.
4-nitro-benzoic acid
62-23-7

4-nitro-benzoic acid

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With thionyl chloride In ethyl acetate for 2h; Heating;100%
With thionyl chloride for 1h; Reflux;100%
With thionyl chloride; N,N-dimethyl-formamide for 5h; Reflux;100%
bis(trichloromethyl) carbonate
32315-10-9

bis(trichloromethyl) carbonate

4-nitro-benzoic acid
62-23-7

4-nitro-benzoic acid

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With pyridine; triethylamine In toluene at 0 - 20℃; for 20h;90%
5-fluorouracil
51-21-8

5-fluorouracil

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
52.9%
potassium 4-nitrobenzoate
15922-01-7

potassium 4-nitrobenzoate

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With thionyl chloride; N,N-dimethyl-formamide at 70 - 75℃; for 0.5h;98.5%
oxalyl dichloride
79-37-8

oxalyl dichloride

RT

RT

4-nitro-benzoic acid
62-23-7

4-nitro-benzoic acid

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
In dichloromethane; N,N-dimethyl-formamide; benzene
4-nitrobenzaldehdye
555-16-8

4-nitrobenzaldehdye

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With iron(III) chloride; Benzotrichlorid In benzene at 60℃; Rate constant; Mechanism; Thermodynamic data; various concentration ratios;
With trichloroisocyanuric acid In dichloromethane at 20℃; for 120h; Inert atmosphere;
With trichloroisocyanuric acid In dichloromethane at 20℃; for 4h; Inert atmosphere; Irradiation;
With N-chloro-succinimide; thio-xanthene-9-one In acetonitrile at 20℃; for 7h; Irradiation;
N-amino-(4-nitrophenyl)carboxamide
636-97-5

N-amino-(4-nitrophenyl)carboxamide

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With hydrogenchloride; Nitroethane; chlorine
oxalyl dichloride
79-37-8

oxalyl dichloride

sodium-4-nitro benzoate

sodium-4-nitro benzoate

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With benzene
4-nitrobenzyl chloride
619-73-8

4-nitrobenzyl chloride

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With trichloroisocyanuric acid In dichloromethane at 20℃; for 120h; Inert atmosphere;
tert-butyl 4-nitrobenzoate
19756-72-0

tert-butyl 4-nitrobenzoate

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With thionyl chloride; water In toluene at 100℃; for 16h; Sealed tube;
p-nitrobenzene iodide
636-98-6

p-nitrobenzene iodide

aroyl chloride

aroyl chloride

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In toluene at 100℃; for 12h;
tert-butyl 4-nitrobenzoate
19756-72-0

tert-butyl 4-nitrobenzoate

A

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

B

tert-butyl alcohol
75-65-0

tert-butyl alcohol

Conditions
ConditionsYield
With sodium hydroxide at 25℃; Rate constant; Equilibrium constant;
trans-5-methyl-2-cyclohexen-p-nitrobenzoate
52393-62-1, 92248-91-4, 99659-46-8

trans-5-methyl-2-cyclohexen-p-nitrobenzoate

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With water
(p-nitrophenyl)chlorocarbene
102146-13-4

(p-nitrophenyl)chlorocarbene

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With oxygen In 1,1,2-Trichloro-1,2,2-trifluoroethane at 20℃; Kinetics; Further Variations:; Temperatures;
pyridine
110-86-1

pyridine

4-nitro-benzoic acid
62-23-7

4-nitro-benzoic acid

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With thionyl chloride; diethyl ether
benzoyl chloride
98-88-4

benzoyl chloride

A

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

B

m-nitrobenzoic acid chloride
121-90-4

m-nitrobenzoic acid chloride

Conditions
ConditionsYield
With tetrachloromethane; phosphorus pentaoxide; dinitrogen pentoxide
Dichloromethyl methyl ether
4885-02-3

Dichloromethyl methyl ether

4-nitro-benzoic acid
62-23-7

4-nitro-benzoic acid

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With zinc(II) chloride
oxalyl dichloride
79-37-8

oxalyl dichloride

4-nitro-benzoic acid
62-23-7

4-nitro-benzoic acid

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

oxalyl dichloride
79-37-8

oxalyl dichloride

4-nitro-benzoic acid
62-23-7

4-nitro-benzoic acid

A

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

B

<4-nitro-benzoic acid >-anhydride

<4-nitro-benzoic acid >-anhydride

C

oxalic acid bis-<4-nitro-benzoic acid >-anhydride

oxalic acid bis-<4-nitro-benzoic acid >-anhydride

3-chloro-3-(p-nitrophenyl)diazirine
39184-67-3

3-chloro-3-(p-nitrophenyl)diazirine

A

4-nitrobenzaldehdye
555-16-8

4-nitrobenzaldehdye

B

4-nitrobenzyl chloride
100-14-1

4-nitrobenzyl chloride

C

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With oxygen In 2,2,4-trimethylpentane Product distribution; Mechanism; Ambient temperature; Irradiation;
1-methyl-4-nitrobenzene
99-99-0

1-methyl-4-nitrobenzene

P2O5

P2O5

A

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

B

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
at 180℃; Einleiten von Chlor;
1-methyl-4-nitrobenzene
99-99-0

1-methyl-4-nitrobenzene

phosphorus pentachloride
10026-13-8, 874483-75-7

phosphorus pentachloride

A

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

B

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
at 180℃; Einleiten von Chlor;
tetrachloromethane
56-23-5

tetrachloromethane

benzoyl chloride
98-88-4

benzoyl chloride

nitrogen pentoxide

nitrogen pentoxide

phosphorus pentoxide

phosphorus pentoxide

A

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

B

m-nitrobenzoic acid chloride
121-90-4

m-nitrobenzoic acid chloride

Conditions
ConditionsYield
at -10℃;
4-nitro-benzoic acid
62-23-7

4-nitro-benzoic acid

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With thionyl chloride In ethyl acetate for 2h; Heating;100%
With thionyl chloride for 1h; Reflux;100%
With thionyl chloride; N,N-dimethyl-formamide for 5h; Reflux;100%
potassium 4-nitrobenzoate
15922-01-7

potassium 4-nitrobenzoate

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With thionyl chloride; N,N-dimethyl-formamide at 70 - 75℃; for 0.5h;98.5%
(4-nitrophenyl)ethanone
100-19-6

(4-nitrophenyl)ethanone

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
Stage #1: (4-nitrophenyl)ethanone With pyridine; disulfur dichloride In chlorobenzene at 20℃; for 2.5h;
Stage #2: With sulfuryl dichloride In chlorobenzene at 20 - 132℃; for 21h; Reagent/catalyst; Temperature;
90%
Stage #1: (4-nitrophenyl)ethanone With pyridine; sulfur monochloride In chlorobenzene at 20℃;
Stage #2: With thionyl chloride In chlorobenzene at 20 - 132℃;
71%
With pyridine; disulfur dichloride at 70 - 138℃; for 21.5h;83 %Spectr.
bis(trichloromethyl) carbonate
32315-10-9

bis(trichloromethyl) carbonate

4-nitro-benzoic acid
62-23-7

4-nitro-benzoic acid

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With pyridine; triethylamine In toluene at 0 - 20℃; for 20h;90%
5-fluorouracil
51-21-8

5-fluorouracil

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
52.9%
pyridine
110-86-1

pyridine

4-nitro-benzoic acid
62-23-7

4-nitro-benzoic acid

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With thionyl chloride; diethyl ether
benzoyl chloride
98-88-4

benzoyl chloride

A

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

B

m-nitrobenzoic acid chloride
121-90-4

m-nitrobenzoic acid chloride

Conditions
ConditionsYield
With tetrachloromethane; phosphorus pentaoxide; dinitrogen pentoxide
N-amino-(4-nitrophenyl)carboxamide
636-97-5

N-amino-(4-nitrophenyl)carboxamide

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With hydrogenchloride; Nitroethane; chlorine
oxalyl dichloride
79-37-8

oxalyl dichloride

4-nitro-benzoic acid
62-23-7

4-nitro-benzoic acid

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Dichloromethyl methyl ether
4885-02-3

Dichloromethyl methyl ether

4-nitro-benzoic acid
62-23-7

4-nitro-benzoic acid

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With zinc(II) chloride
tert-butyl 4-nitrobenzoate
19756-72-0

tert-butyl 4-nitrobenzoate

A

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

B

tert-butyl alcohol
75-65-0

tert-butyl alcohol

Conditions
ConditionsYield
With sodium hydroxide at 25℃; Rate constant; Equilibrium constant;
trans-5-methyl-2-cyclohexen-p-nitrobenzoate
52393-62-1, 92248-91-4, 99659-46-8

trans-5-methyl-2-cyclohexen-p-nitrobenzoate

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With water
4-nitrobenzaldehdye
555-16-8

4-nitrobenzaldehdye

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With iron(III) chloride; Benzotrichlorid In benzene at 60℃; Rate constant; Mechanism; Thermodynamic data; various concentration ratios;
With trichloroisocyanuric acid In dichloromethane at 20℃; for 120h; Inert atmosphere;
With trichloroisocyanuric acid In dichloromethane at 20℃; for 4h; Inert atmosphere; Irradiation;
With N-chloro-succinimide; thio-xanthene-9-one In acetonitrile at 20℃; for 7h; Irradiation;
3-chloro-3-(p-nitrophenyl)diazirine
39184-67-3

3-chloro-3-(p-nitrophenyl)diazirine

A

4-nitrobenzaldehdye
555-16-8

4-nitrobenzaldehdye

B

4-nitrobenzyl chloride
100-14-1

4-nitrobenzyl chloride

C

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With oxygen In 2,2,4-trimethylpentane Product distribution; Mechanism; Ambient temperature; Irradiation;
oxalyl dichloride
79-37-8

oxalyl dichloride

sodium-4-nitro benzoate

sodium-4-nitro benzoate

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With benzene
tetrachloromethane
56-23-5

tetrachloromethane

benzoyl chloride
98-88-4

benzoyl chloride

nitrogen pentoxide

nitrogen pentoxide

phosphorus pentoxide

phosphorus pentoxide

A

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

B

m-nitrobenzoic acid chloride
121-90-4

m-nitrobenzoic acid chloride

Conditions
ConditionsYield
at -10℃;
oxalyl dichloride
79-37-8

oxalyl dichloride

4-nitro-benzoic acid
62-23-7

4-nitro-benzoic acid

A

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

B

<4-nitro-benzoic acid >-anhydride

<4-nitro-benzoic acid >-anhydride

C

oxalic acid bis-<4-nitro-benzoic acid >-anhydride

oxalic acid bis-<4-nitro-benzoic acid >-anhydride

1-methyl-4-nitrobenzene
99-99-0

1-methyl-4-nitrobenzene

phosphorus pentachloride
10026-13-8, 874483-75-7

phosphorus pentachloride

A

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

B

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
at 180℃; Einleiten von Chlor;
1-methyl-4-nitrobenzene
99-99-0

1-methyl-4-nitrobenzene

P2O5

P2O5

A

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

B

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
at 180℃; Einleiten von Chlor;
(p-nitrophenyl)chlorocarbene
102146-13-4

(p-nitrophenyl)chlorocarbene

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With oxygen In 1,1,2-Trichloro-1,2,2-trifluoroethane at 20℃; Kinetics; Further Variations:; Temperatures;
oxalyl dichloride
79-37-8

oxalyl dichloride

RT

RT

4-nitro-benzoic acid
62-23-7

4-nitro-benzoic acid

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
In dichloromethane; N,N-dimethyl-formamide; benzene
4-nitrobenzyl chloride
619-73-8

4-nitrobenzyl chloride

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With trichloroisocyanuric acid In dichloromethane at 20℃; for 120h; Inert atmosphere;
tert-butyl 4-nitrobenzoate
19756-72-0

tert-butyl 4-nitrobenzoate

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With thionyl chloride; water In toluene at 100℃; for 16h; Sealed tube;
p-nitrobenzene iodide
636-98-6

p-nitrobenzene iodide

aroyl chloride

aroyl chloride

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In toluene at 100℃; for 12h;
isobutylamine
78-81-9

isobutylamine

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

N-isobutyl-4-nitrobenzamide
2585-25-3

N-isobutyl-4-nitrobenzamide

Conditions
ConditionsYield
With triethylamine In benzene100%
With triethylamine In chloroform78%
4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

aniline
62-53-3

aniline

4-nitrobenzanilide
3460-11-5

4-nitrobenzanilide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 2.5h;100%
With pyridine Reflux;95%
With pyridine at 20℃; Inert atmosphere; Reflux;91%
4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

benzyl alcohol
100-51-6

benzyl alcohol

benzyl 4-nitrobenzoate
14786-27-7

benzyl 4-nitrobenzoate

Conditions
ConditionsYield
With dmap In dichloromethane at 20℃; for 96h; Inert atmosphere;100%
With dmap In dichloromethane at 20℃; for 24h;92%
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 1h; Inert atmosphere;82%
4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

recorcinol
108-46-3

recorcinol

3-(4-nitrobenzoyloxy)phenyl 4-nitrobenzoate
187264-29-5

3-(4-nitrobenzoyloxy)phenyl 4-nitrobenzoate

Conditions
ConditionsYield
With pyridine In tetrahydrofuran at 20℃; for 24h;100%
With tetralin at 160℃;
With pyridine at 100℃;
With pyridine In toluene Heating;
(-)-kainic acid
487-79-6

(-)-kainic acid

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

[(3S)-2t-carboxy-4c-isopropenyl-1-(4-nitro-benzoyl)-pyrrolidin-3r-yl]-acetic acid
101575-64-8

[(3S)-2t-carboxy-4c-isopropenyl-1-(4-nitro-benzoyl)-pyrrolidin-3r-yl]-acetic acid

Conditions
ConditionsYield
With sodium hydroxide In water at 0 - 20℃; for 20h; Inert atmosphere;100%
With water; sodium carbonate
3-hydroxymethyl-3-methyloxethane
3143-02-0

3-hydroxymethyl-3-methyloxethane

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

(3-methyloxetan-3-yl)methyl 4-nitrobenzoate
140635-77-4

(3-methyloxetan-3-yl)methyl 4-nitrobenzoate

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 20℃; for 0.333333h;100%
L-glutamic acid 5-tert-butyl 1-methyl ester hydrochloride
6234-01-1

L-glutamic acid 5-tert-butyl 1-methyl ester hydrochloride

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

α-methyl γ-tert-butyl N-(p-nitrobenzoyl)-L-glutamate
95485-03-3

α-methyl γ-tert-butyl N-(p-nitrobenzoyl)-L-glutamate

Conditions
ConditionsYield
With triethylamine In dichloromethane for 18h;100%
tetramethylstannane
594-27-4

tetramethylstannane

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

(4-nitrophenyl)ethanone
100-19-6

(4-nitrophenyl)ethanone

Conditions
ConditionsYield
With bis(η3-allyl-μ-chloropalladium(II)) In N,N,N,N,N,N-hexamethylphosphoric triamide at 20℃; for 0.166667h; Mechanism;100%
With bis(η3-allyl-μ-chloropalladium(II)) In N,N,N,N,N,N-hexamethylphosphoric triamide at 20℃; for 0.166667h;100%
With benzoylchlorobis(triphenylphosphine)palladium(II) In chloroform at 65℃; for 24h;95%
With N,N,N,N,N,N-hexamethylphosphoric triamide; poly-γ-(diphenylphosphino)propylsiloxane palladium(0) at 65℃; for 20h;83%
4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

1-(2-oxazolinyl)indole
140934-56-1

1-(2-oxazolinyl)indole

N-(2-Chloro-ethyl)-N-(indole-1-carbonyl)-4-nitro-benzamide

N-(2-Chloro-ethyl)-N-(indole-1-carbonyl)-4-nitro-benzamide

Conditions
ConditionsYield
In benzene for 12h; Heating;100%
4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

2,3,6-tridesoxy-3-(trifluoroacetamido)-L-ribo-hex-1-enitol
73891-06-2

2,3,6-tridesoxy-3-(trifluoroacetamido)-L-ribo-hex-1-enitol

2,3,6-tridesoxy-4-O-p-nitrobenzoyl-3-(trifluoroacetamido)-L-ribo-hex-1-enitol
73891-07-3

2,3,6-tridesoxy-4-O-p-nitrobenzoyl-3-(trifluoroacetamido)-L-ribo-hex-1-enitol

Conditions
ConditionsYield
In pyridine at 20℃; for 16h;100%
4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

methyl 5-O-benzoyl-3-O-benzyl-β-D-ribofuranoside
101024-28-6

methyl 5-O-benzoyl-3-O-benzyl-β-D-ribofuranoside

methyl 5-O-benzoyl-3-O-benzyl-2-O-(p-nitrobenzoyl)-β-D-ribofuranoside
101024-29-7

methyl 5-O-benzoyl-3-O-benzyl-2-O-(p-nitrobenzoyl)-β-D-ribofuranoside

Conditions
ConditionsYield
With pyridine for 18h; Ambient temperature;100%
4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

methyl 5-O-benzoyl-2-O-benzyl-β-D-ribofuranoside
101024-26-4

methyl 5-O-benzoyl-2-O-benzyl-β-D-ribofuranoside

methyl 5-O-benzoyl-2-O-benzyl-3-O-(p-nitrobenzoyl)-β-D-ribofuranoside
101024-27-5

methyl 5-O-benzoyl-2-O-benzyl-3-O-(p-nitrobenzoyl)-β-D-ribofuranoside

Conditions
ConditionsYield
With pyridine for 18h; Ambient temperature;100%
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