2-(azidomethyl)pyridine(SALTDATA: FREE)

Base Information

• Chemical Name: 2-(azidomethyl)pyridine(SALTDATA: FREE)
• CAS No.: 609770-35-6
• Molecular Formula: C6H6N4
• Molecular Weight: 134.14
• Hs Code.: 2933399090
• Mol file: 609770-35-6.mol

Synonyms:2-(3-CHLORO-PHENYL)-PYRIDIN-3-YLAMINE;2-methylpyridineazide;benzyl 2-azidomethylpyridine;picolyl azide;Pyridine,2-(azidomethyl);I02-4858;2-picolylazide;

Chemical Property of 2-(azidomethyl)pyridine(SALTDATA: FREE)

Chemical Property:

• PSA: 62.64000
• LogP: 1.34466

Purity/Quality:

98%min ^*data from raw suppliers

2-(azidomethyl)pyridine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(azidomethyl)pyridine(SALTDATA: FREE)

There total 1 articles about 2-(azidomethyl)pyridine(SALTDATA: FREE) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2-chloromethylpyridine (4377-33-7) → 2-azidomethylpyridine (609770-35-6)

Guidance literature:

With sodium azide; sodium iodide; In acetonitrile; for 24h; Reflux;

DOI:10.1039/c4ob01176g

Reference yield: 100.0%

2-azidomethylpyridine (609770-35-6) + tetrakis(actonitrile)copper(I) hexafluorophosphate (64443-05-6) + zinc(II)-5-(4-ethynylphenyl)-15-(2,4,6-trimethylphenyl)porphyrin + 2,9-dimesityl-[1,10]-phenanthroline (192226-54-3) → C43H32N8Zn*C30H28N2*Cu(1+)*F6P(1-)

Guidance literature:

In chloroform-d1; dichloromethane-d2; at 50 ℃; for 24h;

DOI:10.1039/d1cc02805g

Reference yield: 100.0%

2-azidomethylpyridine (609770-35-6) + tetrakis(actonitrile)copper(I) hexafluorophosphate (64443-05-6) + (((CH3)3C6H2)2C20H8N4(C6H4C2C12H5N2(C6H2(CH3)3)(C6(CH3)4Br))2)Zn (924272-92-4) + zinc(II)-5-(4-ethynylphenyl)-15-(2,4,6-trimethylphenyl)porphyrin + 4,4'-((((2,3,5,6-tetramethyl-1,4-phenylene)bis(ethyn-2,1-diyl))bis(3,1-phenylene))bis(ethyn-2,1-diyl))dipyridine → C116H94Br2N8Zn*C40H28N2*2Cu(1+)*2F6P(1-)*2C43H32N8Zn

Guidance literature:

In chloroform-d1; dichloromethane-d2; at 50 ℃; for 24h;

DOI:10.1039/d1cc02805g

upstream raw materials:

2-chloromethylpyridine

Downstream raw materials:

2-{[4-phenyl-1H-1,2,3-triazol-1-yl]methyl}pyridine

2-(4-methoxyphenyl)-N-((1-(pyridin-2-ylmethyl)-1H-1,2,3-triazol-4-yl)methyl)diazenecarboxamide

2-(4-fluorophenyl)-N-((1-(pyridin-2-ylmethyl)-1H-1,2,3-triazol-4-yl)methyl)diazenecarboxamide

2-(4-nitrophenyl)-N-((1-(pyridin-2-ylmethyl)-1H-1,2,3-triazol-4-yl)methyl)diazenecarboxamide

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