Benzoic acid, 2-methoxy-4-[(phenylmethyl)amino]-, methyl ester

Base Information

Chemical Name:Benzoic acid, 2-methoxy-4-[(phenylmethyl)amino]-, methyl ester
CAS No.:609784-58-9
Molecular Formula:C16H17NO3
Molecular Weight:271.316
Hs Code.:

Synonyms:

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Chemical Property of Benzoic acid, 2-methoxy-4-[(phenylmethyl)amino]-, methyl ester

Chemical Property:

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Technology Process of Benzoic acid, 2-methoxy-4-[(phenylmethyl)amino]-, methyl ester

There total 1 articles about Benzoic acid, 2-methoxy-4-[(phenylmethyl)amino]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 27492-84-8
Methyl 4-amino-2-methoxybenzoate

: 100-52-7
benzaldehyde

: 609784-58-9
methyl 4-(benzylamino)-2-methoxybenzoate

Guidance literature:: Methyl 4-amino-2-methoxybenzoate; benzaldehyde; With acetic acid; In methanol; at 20 ℃; for 0.5h;

With sodium cyanoborohydride; In methanol; at 0 - 20 ℃; for 38h;

Reference yield:

: 609784-58-9
methyl 4-(benzylamino)-2-methoxybenzoate

: 609784-61-4
2-methoxy-4-[(1-methylpiperidin-4-yl)amino]benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methylate; formamide / methanol; DMF (N,N-dimethyl-formamide) / 1.5 h / 70 °C

2: ammonium formate / palladium 10% on activated carbon / ethanol / 3 h / Heating / reflux

3: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 14.5 h / 20 °C

With ammonium formate; sodium methylate; sodium tris(acetoxy)borohydride; formamide; acetic acid; palladium 10% on activated carbon; In methanol; DMF (N,N-dimethyl-formamide); ethanol; 1,2-dichloro-ethane;

Reference yield:

: 609784-58-9
methyl 4-(benzylamino)-2-methoxybenzoate

: 609811-57-6
4-[(1-benzoylpiperidin-4-yl)amino]-2-methoxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium methylate; formamide / methanol; DMF (N,N-dimethyl-formamide) / 1.5 h / 70 °C

2.1: ammonium formate / palladium 10% on activated carbon / ethanol / 3 h / Heating / reflux

3.1: acetic acid / methanol / 0.5 h / 20 °C

3.2: 31 h / 20 °C

With ammonium formate; sodium methylate; formamide; acetic acid; palladium 10% on activated carbon; In methanol; DMF (N,N-dimethyl-formamide); ethanol;