Acetic acid, [[6,7-dichloro-2,3-dihydro-2-(4-hydroxyphenyl)-2-methyl-1-oxo-1H-inden -5-yl]oxy]-

Base Information

Chemical Name:Acetic acid, [[6,7-dichloro-2,3-dihydro-2-(4-hydroxyphenyl)-2-methyl-1-oxo-1H-inden -5-yl]oxy]-
CAS No.:61016-62-4
Molecular Formula:C18H14Cl2O5
Molecular Weight:381.212
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid, [[6,7-dichloro-2,3-dihydro-2-(4-hydroxyphenyl)-2-methyl-1-oxo-1H-inden -5-yl]oxy]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Acetic acid, [[6,7-dichloro-2,3-dihydro-2-(4-hydroxyphenyl)-2-methyl-1-oxo-1H-inden -5-yl]oxy]-

There total 11 articles about Acetic acid, [[6,7-dichloro-2,3-dihydro-2-(4-hydroxyphenyl)-2-methyl-1-oxo-1H-inden -5-yl]oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66015-27-8
[1-oxo-2-(4-methoxyphenyl)-2-methyl-6,7-dichloro-5-indanyloxy]acetic acid

: 61016-62-4
[1-Oxo-2-(4-hydroxyphenyl)-2-methyl-6,7-dichloro-5-indanyloxy]acetic acid

Guidance literature:: With hydrogen bromide; acetic acid; In (2S)-N-methyl-1-phenylpropan-2-amine hydrate;

Reference yield:

: 53107-35-0
2',3',-Dichloro-4'-methoxyisobutyrophenone

: 61016-62-4
[1-Oxo-2-(4-hydroxyphenyl)-2-methyl-6,7-dichloro-5-indanyloxy]acetic acid

Guidance literature:: Multi-step reaction with 9 steps

1: bromine; sodium hydrogensulfite / acetic acid

2: lithium bromide / N,N-dimethyl-formamide

3: (2S)-N-methyl-1-phenylpropan-2-amine hydrate; sulfuric acid

4: pyridine hydrochloride

5: potassium carbonate / N-methyl-acetamide

6: potassium tert-butylate / water; tert-butyl alcohol

7: palladium / ethanol

8: hydrogenchloride; sodium hydroxide; potassium carbonate / N-methyl-acetamide; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; water

9: hydrogen bromide; acetic acid / (2S)-N-methyl-1-phenylpropan-2-amine hydrate

With hydrogenchloride; sodium hydroxide; lithium bromide; potassium tert-butylate; hydrogen bromide; bromine; pyridine hydrochloride; potassium carbonate; sodium hydrogensulfite; acetic acid; palladium; In N-methyl-acetamide; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; ethanol; sulfuric acid; water; acetic acid; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 54196-91-7
6,7-dichloro-5-methoxy-2-methyl-1-indanone

: 61016-62-4
[1-Oxo-2-(4-hydroxyphenyl)-2-methyl-6,7-dichloro-5-indanyloxy]acetic acid

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine hydrochloride

2: potassium carbonate / N-methyl-acetamide

3: potassium tert-butylate / water; tert-butyl alcohol

4: palladium / ethanol

5: hydrogenchloride; sodium hydroxide; potassium carbonate / N-methyl-acetamide; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; water

6: hydrogen bromide; acetic acid / (2S)-N-methyl-1-phenylpropan-2-amine hydrate

With hydrogenchloride; sodium hydroxide; potassium tert-butylate; hydrogen bromide; pyridine hydrochloride; potassium carbonate; acetic acid; palladium; In N-methyl-acetamide; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; ethanol; water; tert-butyl alcohol;