[1-oxo-2-(4-methoxyphenyl)-2-methyl-6,7-dichloro-5-indanyloxy]acetic acid

Base Information

Chemical Name:[1-oxo-2-(4-methoxyphenyl)-2-methyl-6,7-dichloro-5-indanyloxy]acetic acid
CAS No.:66015-27-8
Molecular Formula:C₁₉H₁₆Cl₂O₅
Molecular Weight:395.239
Hs Code.:

Synonyms:[1-oxo-2-(4-methoxyphenyl)-2-methyl-6,7-dichloro-5-indanyloxy]acetic acid

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Chemical Property of [1-oxo-2-(4-methoxyphenyl)-2-methyl-6,7-dichloro-5-indanyloxy]acetic acid

Chemical Property:

Purity/Quality:

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Technology Process of [1-oxo-2-(4-methoxyphenyl)-2-methyl-6,7-dichloro-5-indanyloxy]acetic acid

There total 10 articles about [1-oxo-2-(4-methoxyphenyl)-2-methyl-6,7-dichloro-5-indanyloxy]acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66015-52-9
2-(4-methoxyphenyl)-2-methyl-5-hydroxy-6,7-dichloro-1-indanone

: 105-36-2
ethyl bromoacetate

: 66015-27-8
[1-oxo-2-(4-methoxyphenyl)-2-methyl-6,7-dichloro-5-indanyloxy]acetic acid

Guidance literature:: With hydrogenchloride; sodium hydroxide; potassium carbonate; In N-methyl-acetamide; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; water;

Reference yield:

: 53107-35-0
2',3',-Dichloro-4'-methoxyisobutyrophenone

: 66015-27-8
[1-oxo-2-(4-methoxyphenyl)-2-methyl-6,7-dichloro-5-indanyloxy]acetic acid

Guidance literature:: Multi-step reaction with 8 steps

1: bromine; sodium hydrogensulfite / acetic acid

2: lithium bromide / N,N-dimethyl-formamide

3: (2S)-N-methyl-1-phenylpropan-2-amine hydrate; sulfuric acid

4: pyridine hydrochloride

5: potassium carbonate / N-methyl-acetamide

6: potassium tert-butylate / water; tert-butyl alcohol

7: palladium / ethanol

8: hydrogenchloride; sodium hydroxide; potassium carbonate / N-methyl-acetamide; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; water

With hydrogenchloride; sodium hydroxide; lithium bromide; potassium tert-butylate; bromine; pyridine hydrochloride; potassium carbonate; sodium hydrogensulfite; palladium; In N-methyl-acetamide; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; ethanol; sulfuric acid; water; acetic acid; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 54196-91-7
6,7-dichloro-5-methoxy-2-methyl-1-indanone

: 66015-27-8
[1-oxo-2-(4-methoxyphenyl)-2-methyl-6,7-dichloro-5-indanyloxy]acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine hydrochloride

2: potassium carbonate / N-methyl-acetamide

3: potassium tert-butylate / water; tert-butyl alcohol

4: palladium / ethanol

5: hydrogenchloride; sodium hydroxide; potassium carbonate / N-methyl-acetamide; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; water

With hydrogenchloride; sodium hydroxide; potassium tert-butylate; pyridine hydrochloride; potassium carbonate; palladium; In N-methyl-acetamide; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; ethanol; water; tert-butyl alcohol;