2-Formyl-4-methylbenzoic acid

Base Information

Chemical Name:2-Formyl-4-methylbenzoic acid
CAS No.:61099-10-3
Molecular Formula:C9H8O3
Molecular Weight:164.161
Hs Code.:2918300090
DSSTox Substance ID:DTXSID60711443
Wikidata:Q82647094

Synonyms:2-Formyl-4-methylbenzoic acid;61099-10-3;SCHEMBL1795086;DTXSID60711443;AKOS006372745;CS-0345255;EN300-330166;A929587

Suppliers and Price of 2-Formyl-4-methylbenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-Formyl-4-methylbenzoic acid

Chemical Property:

Boiling Point:341.1±30.0 °C(Predicted)
PSA：54.37000
Density:1.263±0.06 g/cm3(Predicted)
LogP:1.50570
XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:164.047344113
Heavy Atom Count:12
Complexity:188

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1)C(=O)O)C=O

Technology Process of 2-Formyl-4-methylbenzoic acid

There total 5 articles about 2-Formyl-4-methylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 7697-27-0
2-bromo-4-methylbenzoic acid

: 61099-10-3
4-methyl-2-formylbenzoic acid

Guidance literature:: 2-bromo-4-methylbenzoic acid; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2018.03.024

Reference yield:

: 54120-64-8
5-methylphthalide

: 61099-10-3
4-methyl-2-formylbenzoic acid

Guidance literature:: 5-methylphthalide; With potassium hydroxide; In methanol; for 1.5h; Reflux; Inert atmosphere;

With manganese(IV) oxide; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1021/ol5031603

Reference yield:

: 72985-23-0
6-methylisobenzofuran-1(3H)-one

: 61099-10-3
4-methyl-2-formylbenzoic acid

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; at 0 ℃; for 3h; Reflux; Inert atmosphere;
DOI:10.1055/s-0033-1338742