2-Benzylspiro[cyclopropane-1,2'-indene]-1',3'-dione

Base Information

Chemical Name:2-Benzylspiro[cyclopropane-1,2'-indene]-1',3'-dione
CAS No.:61124-68-3
Molecular Formula:C18H14O2
Molecular Weight:262.308
Hs Code.:
DSSTox Substance ID:DTXSID30513890

Synonyms:2-Benzylspiro[cyclopropane-1,2'-indene]-1',3'-dione;61124-68-3;DTXSID30513890

Suppliers and Price of 2-Benzylspiro[cyclopropane-1,2'-indene]-1',3'-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-Benzylspiro[cyclopropane-1,2'-indene]-1',3'-dione

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:262.099379685
Heavy Atom Count:20
Complexity:409

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C(C12C(=O)C3=CC=CC=C3C2=O)CC4=CC=CC=C4

Technology Process of 2-Benzylspiro[cyclopropane-1,2'-indene]-1',3'-dione

There total 4 articles about 2-Benzylspiro[cyclopropane-1,2'-indene]-1',3'-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 61124-62-7
1,1-phthaloyl-2-benzoylcyclopropane

: 61124-68-3
2-benzylspiroindene>-1',3'-dione

Guidance literature:: With triethylsilane; trifluoroacetic acid; at 50 ℃; for 6h;

Reference yield: 46.0%

: 300-57-2,57807-91-7
allylbenzene

: 1807-49-4
2-diazo-indan-1,3-dione

: 61124-68-3
2-benzylspiroindene>-1',3'-dione

Guidance literature:: With rhodium(II) acetate; at 90 - 105 ℃; for 3.5h;
DOI:10.1021/jo00247a007

Reference yield: 15.0%

: 300-57-2,57807-91-7
allylbenzene

: 606-23-5
1H-indene-1,3(2H)-dione

: 61124-68-3
2-benzylspiroindene>-1',3'-dione

Guidance literature:: With N-iodo-succinimide; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere; Irradiation;
DOI:10.1021/acs.joc.6b01163