2-(Chlorocarbonyl)phenyl 4-methylbenzene-1-sulfonate

Base Information

Chemical Name:2-(Chlorocarbonyl)phenyl 4-methylbenzene-1-sulfonate
CAS No.:61153-72-8
Molecular Formula:C14H11ClO4S
Molecular Weight:310.758
Hs Code.:
DSSTox Substance ID:DTXSID70492115
Wikidata:Q82337686

Synonyms:61153-72-8;2-(Chlorocarbonyl)phenyl 4-methylbenzene-1-sulfonate;DTXSID70492115

Suppliers and Price of 2-(Chlorocarbonyl)phenyl 4-methylbenzene-1-sulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(Chlorocarbonyl)phenyl 4-methylbenzene-1-sulfonate

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:310.0066577
Heavy Atom Count:20
Complexity:435

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)OC2=CC=CC=C2C(=O)Cl

Technology Process of 2-(Chlorocarbonyl)phenyl 4-methylbenzene-1-sulfonate

There total 2 articles about 2-(Chlorocarbonyl)phenyl 4-methylbenzene-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82745-72-0
2-(((4-methylphenyl)sulfonyl)oxy)benzoic acid

: 61153-72-8
2-(Tosyloxy)benzoylchlorid

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 0 - 20 ℃; for 4h; Inert atmosphere;
DOI:10.1002/chem.201705710

Reference yield:

: 61153-72-8
2-(Tosyloxy)benzoylchlorid

Guidance literature:: 2-Tosyloxybenzoesaeure, PCl5;

Reference yield:

: 61153-72-8
2-(Tosyloxy)benzoylchlorid

: (E)-2-(tert-butyl)-3-oxo-1-(quinolin-8-ylimino)isoindolin-4-yl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 12 h / 20 °C

2: cobalt(II) aceylacetonate; sodium pivalate; silver carbonate / 2,2,2-trifluoroethanol / 16 h / 100 °C / Schlenk technique

With sodium pivalate; cobalt(II) aceylacetonate; triethylamine; silver carbonate; In dichloromethane; 2,2,2-trifluoroethanol;
DOI:10.1002/chem.201705710