Benzene, 1-iodo-2-(1-methylethenyl)-

Base Information

Chemical Name:Benzene, 1-iodo-2-(1-methylethenyl)-
CAS No.:61161-21-5
Molecular Formula:C9H9I
Molecular Weight:244.075
Hs Code.:
DSSTox Substance ID:DTXSID10465489
Nikkaji Number:J1.898.228E
Wikidata:Q82291476

Synonyms:61161-21-5;Benzene, 1-iodo-2-(1-methylethenyl)-;1-IODO-2-(PROP-1-EN-2-YL)BENZENE;1-iodo-2-prop-1-en-2-ylbenzene;SCHEMBL7765253;DTXSID10465489;2-(1-METHYLETHENYL)-1-IODOBENZENE;E72643

Suppliers and Price of Benzene, 1-iodo-2-(1-methylethenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Benzene, 1-iodo-2-(1-methylethenyl)-

Chemical Property:

PSA：0.00000
LogP:3.32430
XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:243.97490
Heavy Atom Count:10
Complexity:129

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=C)C1=CC=CC=C1I

Technology Process of Benzene, 1-iodo-2-(1-methylethenyl)-

There total 8 articles about Benzene, 1-iodo-2-(1-methylethenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 2142-70-3
2-iodoacetophenone

: 1779-49-3
Methyltriphenylphosphonium bromide

: 61161-21-5
2-(1'-methylethenyl)-1-iodobenzene

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 1h; Schlenk technique; Inert atmosphere;

2-iodoacetophenone; In tetrahydrofuran; for 12h; Schlenk technique; Inert atmosphere;

Reference yield: 89.0%

: 2142-70-3
2-iodoacetophenone

: 61161-21-5
2-(1'-methylethenyl)-1-iodobenzene

Guidance literature:: With potassium tert-butylate; Methyltriphenylphosphonium bromide; In tetrahydrofuran; at 0 - 22 ℃; for 16h; Inert atmosphere; Schlenk technique;
DOI:10.1055/s-0036-1590967

Reference yield: 84.0%

: 7073-70-3
1-bromo-2-isopropenylbenzene

: 61161-21-5
2-(1'-methylethenyl)-1-iodobenzene

Guidance literature:: 1-bromo-2-isopropenylbenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

With iodine; In tetrahydrofuran; hexane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo501383v