1-Chloro-4-(1-diazoethyl)benzene

Base Information

• Chemical Name: 1-Chloro-4-(1-diazoethyl)benzene
• CAS No.: 61185-76-0
• Molecular Formula: C8H7ClN2
• Molecular Weight: 166.61
• DSSTox Substance ID: DTXSID50497002
• Nikkaji Number: J675.303E
• Wikidata: Q82346253

Synonyms:1-Chloro-4-(1-diazoethyl)benzene;61185-76-0;DTXSID50497002

Chemical Property of 1-Chloro-4-(1-diazoethyl)benzene

Chemical Property:

• XLogP3: 2.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 166.0297759
• Heavy Atom Count: 11
• Complexity: 177

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=[N+]=[N-])C1=CC=C(C=C1)Cl

Technology Process of 1-Chloro-4-(1-diazoethyl)benzene

There total 4 articles about 1-Chloro-4-(1-diazoethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

ClC6H4C(N2SO2C6H4CH3)CH3(1-)*Na(1+)=NaClC6H4C(N2SO2C6H4CH3)CH3 + N-phenylbenzohydrazonoyl chloride (15424-14-3) → 1-phenyl-2-(phenyl(tosyl)methylene)hydrazine + 1-(p-chlorophenyl)-1-diazoethane (61185-76-0)

Guidance literature:

In N,N-dimethyl-formamide; at 100 ℃; for 2h;

DOI:10.1080/10426507.2013.865122

Reference yield:

(1-(4-chlorophenyl)ethylidene)hydrazine (40137-41-5) → 1-(p-chlorophenyl)-1-diazoethane (61185-76-0)

Guidance literature:

With manganese(IV) oxide; magnesium sulfate; In dichloromethane; at 0 ℃; for 4h;

DOI:10.1016/S0040-4020(01)90521-6

Reference yield:

p-chloroacetophenone tosylhydrazone (75230-50-1) → 1-(p-chlorophenyl)-1-diazoethane (61185-76-0)

Guidance literature:

With caesium carbonate; In tert-Amyl alcohol; at 80 ℃;

DOI:10.1039/c6cc09445g

upstream raw materials:

(1-(4-chlorophenyl)ethylidene)hydrazine

para-chloroacetophenone

N-phenylbenzohydrazonoyl chloride

p-chloroacetophenone tosylhydrazone

Downstream raw materials:

cis-4-cyano-5-(1,1-diphenylethyl)-4-(methoxycarbonyl)-3-methyl-3-(p-chlorophenyl)-1-pyrazoline

1,2-bis[1-(4-chlorophenyl)ethylidene]hydrazine

4-chlorobenzyl benzoate

4-chlorobenzyl acetate

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