Methyl 5-(benzyloxy)-2-hydroxybenzoate

Base Information

• Chemical Name: Methyl 5-(benzyloxy)-2-hydroxybenzoate
• CAS No.: 61227-22-3
• Molecular Formula: C15H14O4
• Molecular Weight: 258.274
• DSSTox Substance ID: DTXSID30515591
• Wikidata: Q82376534
• Mol file: 61227-22-3.mol

Synonyms:Methyl 5-(benzyloxy)-2-hydroxybenzoate;61227-22-3;methyl 2-hydroxy-5-phenylmethoxybenzoate;methyl 5-benzyloxy-2-hydroxybenzoate;Methyl5-(benzyloxy)-2-hydroxybenzoate;methyl 5-benzyloxysalicylate;SCHEMBL710202;DTXSID30515591;STKBIDZTDFSKEP-UHFFFAOYSA-N;CS-0361881;F97216;5-Benzyloxy-2-hydroxy benzoic acid methyl ester;A1-11636

Chemical Property of Methyl 5-(benzyloxy)-2-hydroxybenzoate

Chemical Property:

• Storage Temp.: 2-8°C
• XLogP3: 3.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 258.08920892
• Heavy Atom Count: 19
• Complexity: 286

Purity/Quality:

99% ^*data from raw suppliers

Methyl 5-(benzyloxy)-2-hydroxybenzoate 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC(=O)C1=C(C=CC(=C1)OCC2=CC=CC=C2)O

Technology Process of Methyl 5-(benzyloxy)-2-hydroxybenzoate

There total 5 articles about Methyl 5-(benzyloxy)-2-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

Methyl 2,5-dihydroxybenzoate (2150-46-1) + benzyl bromide (100-39-0) → methyl 2-hydroxy-5-(phenylmethoxy)benzoate (61227-22-3)

Guidance literature:

With potassium carbonate; In methanol; chloroform; for 4h; Heating;

DOI:10.1016/S0040-4020(01)00257-5

Reference yield: 39.0%

→ methyl 2-hydroxy-5-(phenylmethoxy)benzoate (61227-22-3)

Guidance literature:

Reference yield:

6-benzyloxy-2,2-dimethyl-benzo[1,3]dioxin-4-one (1175095-39-2) → methyl 2-hydroxy-5-(phenylmethoxy)benzoate (61227-22-3)

Guidance literature:

6-benzyloxy-2,2-dimethyl-benzo[1,3]dioxin-4-one; With sodium methylate; In tetrahydrofuran; methanol; at 20 ℃; for 1h;

With hydrogenchloride; In tetrahydrofuran; methanol; water;

upstream raw materials:

Methyl 2,5-dihydroxybenzoate

benzyl bromide

6-benzyloxy-2,2-dimethyl-benzo[1,3]dioxin-4-one

2,5-dihydroxybenzoic acid.

Downstream raw materials:

α-[(2-carboxy-4-benzyloxyphenyl)oxy]-γ-butyrolactone

5-Benzyloxy-2-(2-trimethylsilanyl-ethoxymethoxy)-benzoic acid methyl ester

methyl 2-(2-methoxy-2-oxoethoxy)-5-(phenylmethoxy)benzoate

1,11-bis(4'-benzyloxy-2'-methoxycarbonylphenoxy)-3,6,9-trioxaundecane

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