3-Bromo-2-methyl-5-phenylthiophene

Base Information

Chemical Name:3-Bromo-2-methyl-5-phenylthiophene
CAS No.:61285-25-4
Molecular Formula:C11H9BrS
Molecular Weight:253.162
Hs Code.:
DSSTox Substance ID:DTXSID30358526
Nikkaji Number:J1.346.808G
Wikidata:Q82139154

Synonyms:3-bromo-2-methyl-5-phenylthiophene;61285-25-4;SCHEMBL6812091;DTXSID30358526;2-methyl-3-bromo-5-phenyl-thiophene

Suppliers and Price of 3-Bromo-2-methyl-5-phenylthiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 3-Bromo-2-methyl-5-phenylthiophene

Chemical Property:

PSA：28.24000
LogP:4.48600
XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:251.96083
Heavy Atom Count:13
Complexity:166

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C(S1)C2=CC=CC=C2)Br

Technology Process of 3-Bromo-2-methyl-5-phenylthiophene

There total 11 articles about 3-Bromo-2-methyl-5-phenylthiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 29421-73-6
3,5-dibromo-2-methylthiophene

: 98-80-6
phenylboronic acid

: 61285-25-4
3-bromo-2-methyl-5-phenylthiophene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In water; toluene; at 100 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c5nj01718a

Reference yield: 94.0%

: 591-50-4
iodobenzene

: 154566-69-5
3-bromo-2-methylthiophene-5-boronic acid

: 61285-25-4
3-bromo-2-methyl-5-phenylthiophene

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate; In tetrahydrofuran; water; at 80 ℃; Schlenk technique; Inert atmosphere;
DOI:10.3762/bjoc.12.106

Reference yield: 90.0%

: 591-50-4
iodobenzene

: 1310404-98-8
2-(4-bromo-5-methylthiophen-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 61285-25-4
3-bromo-2-methyl-5-phenylthiophene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; at 70 ℃; Inert atmosphere;
DOI:10.1002/asia.201500328