3-Iodo-2-methyl-5-phenylthiophene

Base Information

Chemical Name:3-Iodo-2-methyl-5-phenylthiophene
CAS No.:61285-28-7
Molecular Formula:C11H9IS
Molecular Weight:300.163
Hs Code.:
DSSTox Substance ID:DTXSID80361025
Nikkaji Number:J3.114.202D
Wikidata:Q82143114

Synonyms:3-iodo-2-methyl-5-phenylthiophene;61285-28-7;DTXSID80361025

Suppliers and Price of 3-Iodo-2-methyl-5-phenylthiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-Iodo-2-methyl-5-phenylthiophene

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:299.94697
Heavy Atom Count:13
Complexity:166

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C(S1)C2=CC=CC=C2)I

Technology Process of 3-Iodo-2-methyl-5-phenylthiophene

There total 2 articles about 3-Iodo-2-methyl-5-phenylthiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 61285-25-4
3-bromo-2-methyl-5-phenylthiophene

: 61285-28-7
3-iodo-2-methyl-5-phenylthiophene

Guidance literature:: 3-bromo-2-methyl-5-phenylthiophene; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 0.5h;

With iodine; In diethyl ether; hexane; at -78 - 20 ℃; Further stages.;
DOI:10.1002/anie.200703034

Reference yield:

: 61285-28-7
3-iodo-2-methyl-5-phenylthiophene

Guidance literature:: Bromthiophen 3, Butyllithium, I2;

Reference yield: 93.0%

: 61285-28-7
3-iodo-2-methyl-5-phenylthiophene

: 1066-54-2
trimethylsilylacetylene

: 1010734-29-8
trimethyl(2-(2-methyl-5-phenylthiophen-3-yl)ethynyl)silane

Guidance literature:: With copper(l) iodide; diisopropylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride; at 70 ℃; for 18h;
DOI:10.1002/anie.200703034