2-Chlorobenzaldehyde dimethyl hydrazone

Base Information

• Chemical Name: 2-Chlorobenzaldehyde dimethyl hydrazone
• CAS No.: 5051-47-8
• Molecular Formula: C9H11ClN2
• Molecular Weight: 182.653
• NSC Number: 148442
• Nikkaji Number: J315.316I

Synonyms:5051-47-8;NSC148442;2-Chlorobenzaldehyde dimethyl hydrazone;NSC-148442

Chemical Property of 2-Chlorobenzaldehyde dimethyl hydrazone

Chemical Property:

• Vapor Pressure: 0.00212mmHg at 25°C
• Boiling Point: 290°Cat760mmHg
• Flash Point: 129.2°C
• Density: 1.06g/cm³
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 182.0610761
• Heavy Atom Count: 12
• Complexity: 157

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)N=CC1=CC=CC=C1Cl
• Isomeric SMILES: CN(C)/N=C\C1=CC=CC=C1Cl

Technology Process of 2-Chlorobenzaldehyde dimethyl hydrazone

There total 3 articles about 2-Chlorobenzaldehyde dimethyl hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2-chloro-benzaldehyde (89-98-5) + N,N-Dimethylhydrazine (57-14-7) → 2-chlorobenzaldehyde dimethylhydrazone (5051-47-8)

Guidance literature:

With magnesium sulfate; In dichloromethane; at 20 ℃; for 10h;

DOI:10.1021/ol2016803

Reference yield:

2-chloro-benzaldehyde (89-98-5) + N,N-Dimethylhydrazine (57-14-7) → N'-[1-(2-Chloro-phenyl)-meth-(Z)-ylidene]-N,N-dimethyl-hydrazine (5051-47-8)

Guidance literature:

for 1h; Heating;

DOI:10.1021/jo00294a040

Reference yield:

→ 2-chlorobenzaldehyde dimethylhydrazone (5051-47-8)

Guidance literature:

entspr. Benzaldehyd, entspr. Hydrazin;

upstream raw materials:

2-chloro-benzaldehyde

N,N-Dimethylhydrazine

Downstream raw materials:

10-methyl-9, 10-dihydro-9-acridinone

1-(2-Chloro-phenyl)-3,3,3-trifluoro-propane-1,2-dione

2-Chlorobenzonitrile

3-(2-Chloro-phenyl)-3-(dimethyl-hydrazono)-1,1,1-trifluoro-propan-2-one

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