But-3-en-1-yl 2-chloro-3-oxobutanoate

Base Information

Chemical Name:But-3-en-1-yl 2-chloro-3-oxobutanoate
CAS No.:61363-96-0
Molecular Formula:C₈H₁₁ClO₃
Molecular Weight:190.627
Hs Code.:
DSSTox Substance ID:DTXSID10493661
Mol file:61363-96-0.mol

Synonyms:61363-96-0;But-3-en-1-yl 2-chloro-3-oxobutanoate;DTXSID10493661

Suppliers and Price of But-3-en-1-yl 2-chloro-3-oxobutanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of But-3-en-1-yl 2-chloro-3-oxobutanoate

Chemical Property:

PSA：43.37000
LogP:1.30210
XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:190.0396719
Heavy Atom Count:12
Complexity:189

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C(C(=O)OCCC=C)Cl

Technology Process of But-3-en-1-yl 2-chloro-3-oxobutanoate

There total 1 articles about But-3-en-1-yl 2-chloro-3-oxobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61363-93-7
3-oxobutyric acid but-3-enyl ester

: 61363-96-0
2-Chloro-3-oxo-butyric acid but-3-enyl ester

Guidance literature:: With sulfuryl dichloride; In chloroform;
DOI:10.1021/jo00428a027

Reference yield:

: 61363-96-0
2-Chloro-3-oxo-butyric acid but-3-enyl ester

: 2028-74-2
p-chlorobenzenediazonium chloride

: 61364-01-0
C₁₂H₁₂Cl₂N₂O₂

Guidance literature:: With sodium acetate; In methanol;
DOI:10.1021/jo00428a027

Reference yield:

: 61363-96-0
2-Chloro-3-oxo-butyric acid but-3-enyl ester

: (6S,14S)-7,15-Bis-(4-chloro-phenyl)-3,11-dioxa-7,8,15,16-tetraaza-tricyclo[12.2.1.1^6,9]octadeca-1⁽¹⁶⁾,8-diene-2,10-dione

Guidance literature:: Multi-step reaction with 3 steps

1: NaOAc / methanol; H₂O / Ambient temperature; pH 5, overnight

2: 5 percent / Ag₂CO₃ / dioxane / 24 h / Ambient temperature

3: Ag₂CO₃ / dioxane / 96 h / Ambient temperature

With sodium acetate; silver carbonate; In 1,4-dioxane; methanol; water;
DOI:10.1016/S0040-4020(98)83021-4