1,1'-Methylenebis(4-methoxy-3-methylbenzene)

Base Information

• Chemical Name: 1,1'-Methylenebis(4-methoxy-3-methylbenzene)
• CAS No.: 61377-15-9
• Molecular Formula: C₁₇H₂₀O₂
• Molecular Weight: 256.345
• DSSTox Substance ID: DTXSID40494141

Synonyms:61377-15-9;1,1'-Methylenebis(4-methoxy-3-methylbenzene);SCHEMBL11282191;DTXSID40494141

Chemical Property of 1,1'-Methylenebis(4-methoxy-3-methylbenzene)

Chemical Property:

• XLogP3: 4.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 256.146329876
• Heavy Atom Count: 19
• Complexity: 240

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C=CC(=C1)CC2=CC(=C(C=C2)OC)C)OC

Technology Process of 1,1'-Methylenebis(4-methoxy-3-methylbenzene)

There total 2 articles about 1,1'-Methylenebis(4-methoxy-3-methylbenzene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 2-methylmethoxybenzene (578-58-5) → 3-methyl-4-methoxybenzyl chloride (60736-71-2) + bis-(4-methoxy-3-methyl-phenyl)-methane (61377-15-9)

Guidance literature:

anschliessendes Einleiten von HCl unterhalb 5grad;

Reference yield:

→ bis-(4-methoxy-3-methyl-phenyl)-methane (61377-15-9)

Guidance literature:

4,4'-Dihydroxy-Verb. (29), NaOH, Dimethylsulfat;

DOI:10.1021/jo00427a023

Reference yield:

bis-(4-methoxy-3-methyl-phenyl)-methane (61377-15-9) → 4,4'-dimethoxy-3,3'-dimethylbenzophenone (116413-55-9)

Guidance literature:

With sodium dichromate; acetic acid;

upstream raw materials:

formaldehyd

2-methylmethoxybenzene

Downstream raw materials:

4,4'-dimethoxy-3,3'-dimethylbenzophenone

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