1,3-Cyclohexadiene-1-carboxylic acid, 5-(acetyloxy)-6-[3-(4-methoxyphenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8- diazabicyclo[3.2.2]non-6-yl]-, 1,1-dimethylethyl ester

Base Information

• Chemical Name: 1,3-Cyclohexadiene-1-carboxylic acid, 5-(acetyloxy)-6-[3-(4-methoxyphenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8- diazabicyclo[3.2.2]non-6-yl]-, 1,1-dimethylethyl ester
• CAS No.: 61377-98-8
• Molecular Formula: C₂₆H₃₀N₂O₇S₂
• Molecular Weight: 546.665

Synonyms:

Chemical Property of 1,3-Cyclohexadiene-1-carboxylic acid, 5-(acetyloxy)-6-[3-(4-methoxyphenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8- diazabicyclo[3.2.2]non-6-yl]-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3-Cyclohexadiene-1-carboxylic acid, 5-(acetyloxy)-6-[3-(4-methoxyphenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8- diazabicyclo[3.2.2]non-6-yl]-, 1,1-dimethylethyl ester

There total 14 articles about 1,3-Cyclohexadiene-1-carboxylic acid, 5-(acetyloxy)-6-[3-(4-methoxyphenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8- diazabicyclo[3.2.2]non-6-yl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.4%

acetic anhydride (108-24-7) + (5S,6S)-5-Hydroxy-6-[(1R,3R,5R)-3-(4-methoxy-phenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8-diaza-bicyclo[3.2.2]non-6-yl]-cyclohexa-1,3-dienecarboxylic acid tert-butyl ester (61377-97-7,79298-62-7,79298-68-3,79298-69-4,79298-70-7,79298-74-1,79299-12-0) → (5S,6S)-5-Acetoxy-6-[(1R,3R,5R)-3-(4-methoxy-phenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8-diaza-bicyclo[3.2.2]non-6-yl]-cyclohexa-1,3-dienecarboxylic acid tert-butyl ester (61377-98-8,79298-63-8,79298-71-8,79355-50-3)

Guidance literature:

With pyridine; for 1h; Ambient temperature;

DOI:10.1016/S0040-4020(01)97960-8

Reference yield: 96.8%

acetic anhydride (108-24-7) + (5S,6S)-5-Hydroxy-6-[(1R,3S,5R)-3-(4-methoxy-phenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8-diaza-bicyclo[3.2.2]non-6-yl]-cyclohexa-1,3-dienecarboxylic acid tert-butyl ester (61377-97-7,79298-62-7,79298-68-3,79298-69-4,79298-70-7,79298-74-1,79299-12-0) → (5S,6S)-5-Acetoxy-6-[(1R,3S,5R)-3-(4-methoxy-phenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8-diaza-bicyclo[3.2.2]non-6-yl]-cyclohexa-1,3-dienecarboxylic acid tert-butyl ester (61377-98-8,79298-63-8,79298-71-8,79355-50-3)

Guidance literature:

With pyridine; for 1h; Ambient temperature;

DOI:10.1016/S0040-4020(01)97960-8

Reference yield: 92.0%

acetic anhydride (108-24-7) + (5S,6S)-5-Hydroxy-6-[(1R,3S,5R)-3-(4-methoxy-phenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8-diaza-bicyclo[3.2.2]non-6-yl]-cyclohexa-1,3-dienecarboxylic acid tert-butyl ester (61377-97-7,79298-62-7,79298-68-3,79298-69-4,79298-70-7,79298-74-1,79299-12-0) → (5S,6S)-5-Acetoxy-6-[(1R,3S,5R)-3-(4-methoxy-phenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8-diaza-bicyclo[3.2.2]non-6-yl]-cyclohexa-1,3-dienecarboxylic acid tert-butyl ester (61377-98-8,79298-63-8,79298-71-8,79355-50-3)

Guidance literature:

With pyridine; for 1h; Ambient temperature;

DOI:10.1016/S0040-4020(01)97960-8

upstream raw materials:

acetic anhydride

(5S,6S)-5-Hydroxy-6-[(1R,3S,5R)-3-(4-methoxy-phenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8-diaza-bicyclo[3.2.2]non-6-yl]-cyclohexa-1,3-dienecarboxylic acid tert-butyl ester

4-carbo-t-butoxyoxepin

(5S,6S)-5-Hydroxy-6-[(1R,3R,5R)-3-(4-methoxy-phenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8-diaza-bicyclo[3.2.2]non-6-yl]-cyclohexa-1,3-dienecarboxylic acid tert-butyl ester

Downstream raw materials:

dl-Gliotoxin

(1RS)-6-((1SR)-2-chloromethyl-6t-hydroxy-cyclohexa-2,4-dien-r-yl)-3ξ-(4-methoxy-phenyl)-8-methyl-2,4-dithia-6,8-diaza-bicyclo[3.2.2]nonane-7,9-dione

7c-hydroxy-4-hydroxymethyl-2ξ-(4-methoxy-phenyl)-13-methyl-(6ac)-7,11-dihydro-6aH-4r,11ac-azaethano-[1,3,5]dithiazepino[5,4-a]indole-5,12-dione

4-benzyloxymethyl-7c-hydroxy-2ξ-(4-methoxy-phenyl)-13-methyl-(6ac)-7,11-dihydro-6aH-4r,11ac-azaethano-[1,3,5]dithiazepino[5,4-a]indole-5,12-dione

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