Isoxazole, 4,5-dihydro-5-methyl-5-(nitromethyl)-3-(4-nitrophenyl)-

Base Information

Chemical Name:Isoxazole, 4,5-dihydro-5-methyl-5-(nitromethyl)-3-(4-nitrophenyl)-
CAS No.:61428-19-1
Molecular Formula:C11H11N3O5
Molecular Weight:265.225
Hs Code.:
DSSTox Substance ID:DTXSID30485740

Synonyms:61428-19-1;Isoxazole, 4,5-dihydro-5-methyl-5-(nitromethyl)-3-(4-nitrophenyl)-;DTXSID30485740

Suppliers and Price of Isoxazole, 4,5-dihydro-5-methyl-5-(nitromethyl)-3-(4-nitrophenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Isoxazole, 4,5-dihydro-5-methyl-5-(nitromethyl)-3-(4-nitrophenyl)-

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:265.06987046
Heavy Atom Count:19
Complexity:406

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CC(=NO1)C2=CC=C(C=C2)[N+](=O)[O-])C[N+](=O)[O-]

Technology Process of Isoxazole, 4,5-dihydro-5-methyl-5-(nitromethyl)-3-(4-nitrophenyl)-

There total 5 articles about Isoxazole, 4,5-dihydro-5-methyl-5-(nitromethyl)-3-(4-nitrophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1606-30-0
1-Nitro-2-methyl-1-propen

: 1011-84-3
4-nitrobenzohydroximoyl chloride

: 61428-19-1
5-methyl-5-nitromethyl-3-(4-nitro-phenyl)-4,5-dihydro-isoxazole

Guidance literature:: In toluene; at 110 ℃;

Reference yield: 75.0%

: 1606-31-1
2-methyl-3-nitro-propene

: 1011-84-3
4-nitrobenzohydroximoyl chloride

: 61428-19-1
5-methyl-5-nitromethyl-3-(4-nitro-phenyl)-4,5-dihydro-isoxazole

Guidance literature:: In toluene; at 110 ℃; for 13h;

Reference yield:

: 1011-84-3
4-nitrobenzohydroximoyl chloride

: 61428-19-1
5-methyl-5-nitromethyl-3-(4-nitro-phenyl)-4,5-dihydro-isoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: TEA / diethyl ether / 0.08 h

2: diethyl ether / 1.) RT, 12 h, 2.) reflux, 2 h

With TEA; In diethyl ether;