[4-(Dichloromethanesulfonyl)-2-nitrophenyl]hydrazine

Base Information

Chemical Name:[4-(Dichloromethanesulfonyl)-2-nitrophenyl]hydrazine
CAS No.:61497-11-8
Molecular Formula:C7H7Cl2N3O4S
Molecular Weight:300.122
Hs Code.:
DSSTox Substance ID:DTXSID20508573
Wikidata:Q82365617

Synonyms:61497-11-8;[4-(Dichloromethanesulfonyl)-2-nitrophenyl]hydrazine;DTXSID20508573

Suppliers and Price of [4-(Dichloromethanesulfonyl)-2-nitrophenyl]hydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of [4-(Dichloromethanesulfonyl)-2-nitrophenyl]hydrazine

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:298.9534323
Heavy Atom Count:17
Complexity:378

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1S(=O)(=O)C(Cl)Cl)[N+](=O)[O-])NN

Technology Process of [4-(Dichloromethanesulfonyl)-2-nitrophenyl]hydrazine

There total 3 articles about [4-(Dichloromethanesulfonyl)-2-nitrophenyl]hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 61496-44-4
4-dichloromethylsulfonyl-2-nitrochlorobenzene

: 61497-11-8
4-dichloromethylsulfonyl-2-nitrophenylhydrazine

Guidance literature:: With hydrazine hydrate; In N,N-dimethyl-formamide; for 1h; Ambient temperature;

Reference yield:

: 32748-30-4
1-chloro-4-((dichloromethyl)sulfonyl)benzene

: 61497-11-8
4-dichloromethylsulfonyl-2-nitrophenylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: conc. H₂SO₄, HNO₃ / 1 h

2: 75 percent / H₂NNH₂*H₂O / dimethylformamide / 1 h / Ambient temperature

With sulfuric acid; nitric acid; hydrazine hydrate; In N,N-dimethyl-formamide;

Reference yield:

: 14752-66-0
sodium p-chlorobenzenesulphinate

: 61497-11-8
4-dichloromethylsulfonyl-2-nitrophenylhydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / aq. NaOH / 8 h / Heating

2: conc. H₂SO₄, HNO₃ / 1 h

3: 75 percent / H₂NNH₂*H₂O / dimethylformamide / 1 h / Ambient temperature

With sodium hydroxide; sulfuric acid; nitric acid; hydrazine hydrate; In N,N-dimethyl-formamide;