Benzene, 1-chloro-4-[(dichloromethyl)sulfonyl]-2-nitro-

Base Information

Chemical Name:Benzene, 1-chloro-4-[(dichloromethyl)sulfonyl]-2-nitro-
CAS No.:61496-44-4
Molecular Formula:C7H4Cl3NO4S
Molecular Weight:304.538
Hs Code.:
DSSTox Substance ID:DTXSID30362507
Wikidata:Q82145645
ChEMBL ID:CHEMBL3358393

Synonyms:61496-44-4;Benzene, 1-chloro-4-[(dichloromethyl)sulfonyl]-2-nitro-;C7H4Cl3NO4S;1-Chloro-4-(dichloro-methanesulfonyl)-2-nitro-benzene;CHEMBL3358393;DTXSID30362507;STK011846;AKOS000538794;1-chloro-4-(dichloromethylsulfonyl)-2-nitro-benzene;1-chloro-4-[(dichloromethyl)sulfonyl]-2-nitrobenzene

Suppliers and Price of Benzene, 1-chloro-4-[(dichloromethyl)sulfonyl]-2-nitro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Benzene, 1-chloro-4-[(dichloromethyl)sulfonyl]-2-nitro-

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:302.892662
Heavy Atom Count:16
Complexity:361

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1S(=O)(=O)C(Cl)Cl)[N+](=O)[O-])Cl

Technology Process of Benzene, 1-chloro-4-[(dichloromethyl)sulfonyl]-2-nitro-

There total 4 articles about Benzene, 1-chloro-4-[(dichloromethyl)sulfonyl]-2-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 32748-30-4
1-chloro-4-((dichloromethyl)sulfonyl)benzene

: 61496-44-4
4-dichloromethylsulfonyl-2-nitrochlorobenzene

Guidance literature:: With sulfuric acid; nitric acid; In water; at 60 - 80 ℃; for 2h;
DOI:10.1016/j.bmc.2014.11.038

Reference yield:

: 14752-66-0
sodium p-chlorobenzenesulphinate

: 61496-44-4
4-dichloromethylsulfonyl-2-nitrochlorobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / aq. NaOH / 8 h / Heating

2: conc. H₂SO₄, HNO₃ / 1 h

With sodium hydroxide; sulfuric acid; nitric acid;

Reference yield:

: 108-90-7
chlorobenzene

: 61496-44-4
4-dichloromethylsulfonyl-2-nitrochlorobenzene

Guidance literature:: Multi-step reaction with 4 steps

1: chlorosulfonic acid / 1 h / 20 °C

2: sodium sulfite / water / 1 h / 80 - 90 °C

3: potassium hydroxide / water / 4 h / Reflux

4: sulfuric acid; nitric acid / water / 2 h / 60 - 80 °C

With chlorosulfonic acid; sulfuric acid; nitric acid; potassium hydroxide; sodium sulfite; In water;
DOI:10.1016/j.bmc.2014.11.038