3-(3-Oxocyclohex-1-en-1-yl)propyl methanesulfonate

Base Information

Chemical Name:3-(3-Oxocyclohex-1-en-1-yl)propyl methanesulfonate
CAS No.:61563-72-2
Molecular Formula:C₁₀H₁₆O₄S
Molecular Weight:232.301
Hs Code.:
DSSTox Substance ID:DTXSID30574401
Wikidata:Q82463426

Synonyms:61563-72-2;3-(3-Oxocyclohex-1-en-1-yl)propyl methanesulfonate;DTXSID30574401

Suppliers and Price of 3-(3-Oxocyclohex-1-en-1-yl)propyl methanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 3-(3-Oxocyclohex-1-en-1-yl)propyl methanesulfonate

Chemical Property:

XLogP3:0.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:232.07693016
Heavy Atom Count:15
Complexity:348

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CS(=O)(=O)OCCCC1=CC(=O)CCC1

Technology Process of 3-(3-Oxocyclohex-1-en-1-yl)propyl methanesulfonate

There total 4 articles about 3-(3-Oxocyclohex-1-en-1-yl)propyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61589-86-4
3-(3-hydroxy-propyl)cyclohex-2-en-1-one

: 124-63-0
methanesulfonyl chloride

: 61563-72-2
Methanesulfonic acid 3-(3-oxo-cyclohex-1-enyl)-propyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 ℃; for 2h;
DOI:10.1021/jo00138a019

Reference yield:

: 5323-87-5
3-Ethoxycyclohex-2-en-1-one

: 61563-72-2
Methanesulfonic acid 3-(3-oxo-cyclohex-1-enyl)-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Mg / 1.) THF, 2.) benzene/THF, room temp., 3 h

2: oxalic acid / methanol / 1.5 h / Ambient temperature

3: triethylamine / tetrahydrofuran / 2 h / 0 °C

With oxalic acid; magnesium; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1021/jo00138a019

Reference yield:

: 82026-09-3
3-<3-(1-ethoxyethoxy)propyl>-2-cyclohexen-1-one

: 61563-72-2
Methanesulfonic acid 3-(3-oxo-cyclohex-1-enyl)-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: oxalic acid / methanol / 1.5 h / Ambient temperature

2: triethylamine / tetrahydrofuran / 2 h / 0 °C

With oxalic acid; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1021/jo00138a019