Cyclohexanamine, N-[(2-iodo-4,5-dimethoxyphenyl)methylene]-

Base Information

Chemical Name:Cyclohexanamine, N-[(2-iodo-4,5-dimethoxyphenyl)methylene]-
CAS No.:61599-78-8
Molecular Formula:C₁₅H₂₀INO₂
Molecular Weight:373.234
Hs Code.:
DSSTox Substance ID:DTXSID90446635

Synonyms:61599-78-8;Cyclohexanamine, N-[(2-iodo-4,5-dimethoxyphenyl)methylene]-;DTXSID90446635

Suppliers and Price of Cyclohexanamine, N-[(2-iodo-4,5-dimethoxyphenyl)methylene]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Cyclohexanamine, N-[(2-iodo-4,5-dimethoxyphenyl)methylene]-

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:373.05388
Heavy Atom Count:19
Complexity:292

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C(=C1)C=NC2CCCCC2)I)OC

Technology Process of Cyclohexanamine, N-[(2-iodo-4,5-dimethoxyphenyl)methylene]-

There total 2 articles about Cyclohexanamine, N-[(2-iodo-4,5-dimethoxyphenyl)methylene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5392-10-9
2-bromo-4,5-dimethoxybenzaldehyde

: 61599-78-8
6-iodo-3,4-dimethoxybenzaldehyde cyclohexylimine

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / 16 h / Dean-Stark; Inert atmosphere; Reflux

2.1: n-butyllithium / hexane; tetrahydrofuran / 0.42 h / -78 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

With n-butyllithium; In tetrahydrofuran; hexane; toluene;
DOI:10.15227/orgsyn.065.0108

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 61599-78-8
6-iodo-3,4-dimethoxybenzaldehyde cyclohexylimine

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / 16 h / Dean-Stark; Inert atmosphere; Reflux

2.1: n-butyllithium / hexane; tetrahydrofuran / 0.42 h / -78 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

With n-butyllithium; In tetrahydrofuran; hexane; toluene;
DOI:10.15227/orgsyn.065.0108