4-Tert-butylcycloheptanone

Base Information

Chemical Name:4-Tert-butylcycloheptanone
CAS No.:5932-62-7
Molecular Formula:C₁₁H₂₀O
Molecular Weight:168.279
Hs Code.:
NSC Number:106333
DSSTox Substance ID:DTXSID60295935
Nikkaji Number:J3.129.727C

Synonyms:4-tert-butylcycloheptanone;4-tert-butylcycloheptan-1-one;5932-62-7;4-(tert-Butyl)cycloheptanone;NSC106333;4-t-butylcycloheptanone;4-tert-butyl-cycloheptan-1-one;DTXSID60295935;AKOS024054456;NSC-106333;EN300-85711;Z1258700175

Suppliers and Price of 4-Tert-butylcycloheptanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 4-Tert-butylcycloheptanone

Chemical Property:

Vapor Pressure:0.0577mmHg at 25°C
Boiling Point:232.9°Cat760mmHg
Flash Point:87.4°C
Density:0.9g/cm³
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:168.151415257
Heavy Atom Count:12
Complexity:164

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)C1CCCC(=O)CC1

Technology Process of 4-Tert-butylcycloheptanone

There total 9 articles about 4-Tert-butylcycloheptanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 98-53-3
4-tercbutyl-cyclohexanone

: 18107-18-1
diazomethyl-trimethyl-silane

: 5932-62-7
4-tert-butylcycloheptanone

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -13 - -10 ℃; for 2.3h;
DOI:10.1016/0040-4039(80)80089-X

Reference yield:

: 80-11-5
N-methyl-N-nitrosotoluene-p-sulfonamide

: 98-53-3
4-tercbutyl-cyclohexanone

: 5932-62-7
4-tert-butylcycloheptanone

Guidance literature:: With potassium hydroxide; In ethanol;
DOI:10.1021/jo01023a541

Reference yield:

: 98-53-3
4-tercbutyl-cyclohexanone

: 5932-62-7
4-tert-butylcycloheptanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; diethyl ether / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.5 h / -78 °C / Inert atmosphere

1.3: Inert atmosphere

2.1: sodium sulfate; silica gel / hexane; tetrahydrofuran; diethyl ether / 0.17 h / Inert atmosphere

With n-butyllithium; silica gel; sodium sulfate; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1002/chem.201201346