2-(1-Phenylethyl)benzaldehyde

Base Information

Chemical Name:2-(1-Phenylethyl)benzaldehyde
CAS No.:61608-90-0
Molecular Formula:C15H14O
Molecular Weight:210.276
Hs Code.:
DSSTox Substance ID:DTXSID60501644

Synonyms:2-(1-Phenylethyl)benzaldehyde;61608-90-0;phenyl(formylphenyl)ethane;SCHEMBL9806332;DTXSID60501644;JXIMXDWYILVTRJ-UHFFFAOYSA-N

Suppliers and Price of 2-(1-Phenylethyl)benzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(1-Phenylethyl)benzaldehyde

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:210.104465066
Heavy Atom Count:16
Complexity:218

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C1=CC=CC=C1)C2=CC=CC=C2C=O

Technology Process of 2-(1-Phenylethyl)benzaldehyde

There total 6 articles about 2-(1-Phenylethyl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: N,N-dimethyl-2,2-diphenylpropanamide

: 61608-90-0
2-(1-phenylethyl)benzaldehyde

Guidance literature:: With sodium hydride; sodium iodide; In tetrahydrofuran; mineral oil; at 85 ℃; for 14h; Inert atmosphere; Sealed tube;
DOI:10.1002/anie.201702512

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1613-90-7
4-methoxy-N-[(E)-phenylmethylidene]aniline

: 2,6-bis(1-phenylethyl)benzaldehyde

: 61608-90-0
2-(1-phenylethyl)benzaldehyde

Guidance literature:: 4-methoxy-N-[(E)-phenylmethylidene]aniline; With (trimethylsilyl)methylmagnesium chloride; Tri(p-tolyl)phosphine; cobalt(II) bromide; In tetrahydrofuran; for 0.5h; Inert atmosphere; Schlenk technique; Cooling with ice;

styrene; In tetrahydrofuran; at 40 ℃; for 12h; Inert atmosphere; Schlenk technique;

With hydrogenchloride; water; In ethyl acetate; at 20 ℃; for 0.5h; Overall yield = 78 mg; regioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201207958

Reference yield:

: 957-51-7
diphenamid

: 61608-90-0
2-(1-phenylethyl)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C

1.2: 2 h / 20 °C

2.1: sodium iodide; sodium hydride / tetrahydrofuran; mineral oil / 14 h / 85 °C / Inert atmosphere; Sealed tube

With n-butyllithium; sodium hydride; diisopropylamine; sodium iodide; In tetrahydrofuran; hexane; mineral oil;
DOI:10.1002/anie.201702512