Hydrazinecarboxamide, 2-(1,5-dimethylhexylidene)-

Base Information

• Chemical Name: Hydrazinecarboxamide, 2-(1,5-dimethylhexylidene)-
• CAS No.: 61652-37-7
• Molecular Formula: C9H19N3O
• Molecular Weight: 185.26700
• DSSTox Substance ID: DTXSID90372809
• Mol file: 61652-37-7.mol

Synonyms:61652-37-7;Hydrazinecarboxamide, 2-(1,5-dimethylhexylidene)-;DTXSID90372809;AKOS004905672

Chemical Property of Hydrazinecarboxamide, 2-(1,5-dimethylhexylidene)-

Chemical Property:

• PSA: 68.47000
• LogP: 2.76160
• XLogP3: 1.7
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 185.152812238
• Heavy Atom Count: 13
• Complexity: 187

Purity/Quality:

99% ^*data from raw suppliers

[(6-METHYLHEPTAN-2-YLIDENE)AMINO]UREA 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)CCCC(=NNC(=O)N)C

Technology Process of Hydrazinecarboxamide, 2-(1,5-dimethylhexylidene)-

There total 6 articles about Hydrazinecarboxamide, 2-(1,5-dimethylhexylidene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

semicarbazide hydrochloride (563-41-7) + Acetic acid (3S,5R,10S,13S,14S,17R)-3-acetoxy-17-hydroxy-17-((S)-1-hydroxy-1,5-dimethyl-hexyl)-4,4,10,14-tetramethyl-1,2,3,4,5,6,10,12,14,15,16,17-dodecahydro-cyclopenta[a]phenanthren-13-ylmethyl ester (75410-54-7) → 6-methyl-heptan-2-one semicarbazone (61652-37-7) + 3β,18-Diacetoxy-4,4,14α-trimethyl-androstan-17-on (6722-82-3)

Guidance literature:

With lead(IV) acetate; sodium acetate; Multistep reaction; 1.) benzene, 4 h; 2.) water;

DOI:10.1248/cpb.33.5214

Reference yield:

6-methyl-hepta-3,5-dien-2-one semicarbazone (90768-50-6) → 6-methyl-heptan-2-one semicarbazone (61652-37-7)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethanol;

DOI:10.1002/hlca.19600430618

Reference yield:

6-Methyl-hept-5-en-2-on (110-93-0,129085-68-3) → 6-methyl-heptan-2-one semicarbazone (61652-37-7)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / 3percent Pd-C / ethanol / 3 h

2: CH₃COONa*3H₂O / H₂O / 20 °C

With hydrogen; sodium acetate; palladium on activated charcoal; In ethanol; water;

DOI:10.1248/cpb.33.5214

upstream raw materials:

6-methylheptan-2-one

6-methyl-hepta-3,5-dien-2-one semicarbazone

semicarbazide hydrochloride

Acetic acid (3S,5R,10S,13S,14S,17R)-3-acetoxy-17-hydroxy-17-((S)-1-hydroxy-1,5-dimethyl-hexyl)-4,4,10,14-tetramethyl-1,2,3,4,5,6,10,12,14,15,16,17-dodecahydro-cyclopenta[a]phenanthren-13-ylmethyl ester