2-(Cyclohexylidenemethyl)pyridine

Base Information

Chemical Name:2-(Cyclohexylidenemethyl)pyridine
CAS No.:70525-40-5
Molecular Formula:C12H15N
Molecular Weight:173.258
Hs Code.:
NSC Number:34069
DSSTox Substance ID:DTXSID40283895
Nikkaji Number:J782.040B

Synonyms:2-(cyclohexylidenemethyl)pyridine;70525-40-5;NSC34069;SCHEMBL8889644;DTXSID40283895;NSC-34069

Suppliers and Price of 2-(Cyclohexylidenemethyl)pyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 2-(Cyclohexylidenemethyl)pyridine

Chemical Property:

Vapor Pressure:0.00429mmHg at 25°C
Boiling Point:287.4°Cat760mmHg
Flash Point:124.1°C
Density:1.034g/cm³
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:173.120449483
Heavy Atom Count:13
Complexity:176

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(=CC2=CC=CC=N2)CC1

Technology Process of 2-(Cyclohexylidenemethyl)pyridine

There total 5 articles about 2-(Cyclohexylidenemethyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 57756-06-6
2-(cyclohexylmethyl)pyridine

: 70525-40-5
2-(cyclohexylidenemethyl)pyridine

Guidance literature:: With 2-bromo-5-methyl thiophene; nickel(II) bromide dimethoxyethane; bis(2,2,6,6-tetramethyl-1-piperidyl)zinc; tetra-(n-butyl)ammonium iodide; trimethylphosphane; In tetrahydrofuran; 1,4-dioxane; toluene; at 85 ℃; for 12h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jacs.9b12706

Reference yield: 47.0%

: ((E)-2-Hepta-1,6-dienyl)-pyridine

: 70525-40-5
2-(cyclohexylidenemethyl)pyridine

: 2-[2-Methyl-cyclopent-(Z)-ylidenemethyl]-pyridine

Guidance literature:: With RhCl(PPh₃)3; In tetrahydrofuran; at 120 ℃; for 48h;
DOI:10.1246/cl.1996.939

Reference yield:

: 1121-60-4
pyridine-2-carbaldehyde

: 7333-51-9
cyclohexyl(triphenyl)phosphonium bromide

: 70525-40-5
2-(cyclohexylidenemethyl)pyridine

Guidance literature:: cyclohexyl(triphenyl)phosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 1h; Inert atmosphere;

pyridine-2-carbaldehyde; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/anie.202007352