3,5-Dichloro-4-hydroxy-N,N-dimethylbenzene-1-sulfonamide

Base Information

• Chemical Name: 3,5-Dichloro-4-hydroxy-N,N-dimethylbenzene-1-sulfonamide
• CAS No.: 61712-32-1
• Molecular Formula: C8H9Cl2NO3S
• Molecular Weight: 270.136
• DSSTox Substance ID: DTXSID50501390
• Nikkaji Number: J1.629.344J
• Wikidata: Q82353737

Synonyms:61712-32-1;3,5-Dichloro-4-hydroxy-N,N-dimethylbenzene-1-sulfonamide;SCHEMBL11646801;DTXSID50501390

Chemical Property of 3,5-Dichloro-4-hydroxy-N,N-dimethylbenzene-1-sulfonamide

Chemical Property:

• XLogP3: 2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 268.9680197
• Heavy Atom Count: 15
• Complexity: 302

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)S(=O)(=O)C1=CC(=C(C(=C1)Cl)O)Cl

Technology Process of 3,5-Dichloro-4-hydroxy-N,N-dimethylbenzene-1-sulfonamide

There total 3 articles about 3,5-Dichloro-4-hydroxy-N,N-dimethylbenzene-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

dimethyl-sulfamic acid 2,6-dichloro-phenyl ester → 2,6-dichloro-N,N-dimethyl-1-phenol-4-sulfonamide (61712-32-1)

Guidance literature:

With aluminium trichloride; at 140 ℃; for 1h;

DOI:10.1016/S0040-4039(01)01893-7

Reference yield:

N,N-dimethyl-4-hydroxybenzenesulfonamide (15020-57-2) → 2,6-dichloro-N,N-dimethyl-1-phenol-4-sulfonamide (61712-32-1)

Guidance literature:

In acetic acid;

Reference yield:

→ 2,6-dichloro-N,N-dimethyl-1-phenol-4-sulfonamide (61712-32-1)

Guidance literature:

3,5-Dichlor-4-hydroxy-benzolsulfonylchlorid 3 (X=Cl), Dimethylamin;

upstream raw materials:

N,N-dimethyl-4-hydroxybenzenesulfonamide

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