DiMethyl-(3-Methyl-pyridin-2-yl)-aMine

Base Information

• Chemical Name: DiMethyl-(3-Methyl-pyridin-2-yl)-aMine
• CAS No.: 61713-46-0
• Molecular Formula: C8H12N2
• Molecular Weight: 136.197

Synonyms:2-Pyridinamine,N,N,3-trimethyl;dimethyl-(3-methyl-pyridin-2-yl)-amine;N,N,3-Trimethyl-2-pyridinamine;3-methyl-2-(N,N-dimethylamino)pyridine;2-Dimethylamino-3-methylpyridine;2-Dimethylamino-3-methylpyridin;

Chemical Property of DiMethyl-(3-Methyl-pyridin-2-yl)-aMine

Chemical Property:

• PSA: 16.13000
• LogP: 1.45600

Purity/Quality:

Dimethyl-(3-methyl-pyridin-2-yl)-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DiMethyl-(3-Methyl-pyridin-2-yl)-aMine

There total 1 articles about DiMethyl-(3-Methyl-pyridin-2-yl)-aMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-picoline-N-oxide (1003-73-2) + N,N,N,N,N,N-hexamethylphosphoric triamide (680-31-9) → 3-Methylpyridine (108-99-6) + 2-dimethylamino-3-methylpyridine (61713-46-0) + 2-dimethylamino-5-methylpyridine (147151-28-8)

Guidance literature:

With PPA; at 230 ℃; for 1h; Yield given. Yields of byproduct given;

Reference yield:

Trimethyl borate (121-43-7,63156-11-6) + 2-dimethylamino-3-methylpyridine (61713-46-0) → 3-hydroxymethyl-2-(N,N-dimethylamino)pyridine (104524-65-4) + 3-[(1H-benzimidazol-2-ylthio)methyl]-N,N-dimethyl-2-pyridinamine

Guidance literature:

With n-butyllithium; dihydrogen peroxide; In tetrahydrofuran; hexane;

upstream raw materials:

3-picoline-N-oxide

N,N,N,N,N,N-hexamethylphosphoric triamide

Downstream raw materials:

3-hydroxymethyl-2-(N,N-dimethylamino)pyridine

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