1-Methyl-1,3,3-triphenyl-1,3-disiletane

Base Information

Chemical Name:1-Methyl-1,3,3-triphenyl-1,3-disiletane
CAS No.:61739-79-5
Molecular Formula:C₂₁H₂₂Si₂
Molecular Weight:330.577
Hs Code.:
DSSTox Substance ID:DTXSID80570650
Nikkaji Number:J1.117.457D
Wikidata:Q82458169

Synonyms:1-Methyl-1,3,3-triphenyl-1,3-disiletane;1-Methyl-1,3,3-triphenyl-1,3-disilacyclobutane;61739-79-5;DTXSID80570650

Suppliers and Price of 1-Methyl-1,3,3-triphenyl-1,3-disiletane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 1-Methyl-1,3,3-triphenyl-1,3-disiletane

Chemical Property:

PSA：0.00000
LogP:3.32740
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:330.12600377
Heavy Atom Count:23
Complexity:361

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si]1(C[Si](C1)(C2=CC=CC=C2)C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of 1-Methyl-1,3,3-triphenyl-1,3-disiletane

There total 2 articles about 1-Methyl-1,3,3-triphenyl-1,3-disiletane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 180744-02-9
diphenylbis<(phenylthio)methyl>silane

: 149-74-6
dichloromethylphenylsilane

: 61739-79-5
1-methyl-1,3,3-triphenyl-1,3-disilacyclobutane

Guidance literature:: With Li naphthalenide; In tetrahydrofuran; 1) -20 deg C, 2) -78 deg C to 0 deg C;
DOI:10.1002/cber.19961290710

Reference yield:

: 80-10-4
diphenylsilyl dichloride

: 61739-79-5
1-methyl-1,3,3-triphenyl-1,3-disilacyclobutane

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / diethyl ether; hexane / -40 deg C to r.t.

2: 42 percent / Li naphthalenide / tetrahydrofuran / 1) -20 deg C, 2) -78 deg C to 0 deg C

With Li naphthalenide; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1002/cber.19961290710