3,5-dimethyl-N-phenyl-1H-pyrazole-4-carboxamide

Base Information

Chemical Name:3,5-dimethyl-N-phenyl-1H-pyrazole-4-carboxamide
CAS No.:61747-76-0
Molecular Formula:C12H13N3O
Molecular Weight:215.255
Hs Code.:
DSSTox Substance ID:DTXSID30443744
Nikkaji Number:J2.524.722A
Wikidata:Q82261686

Synonyms:61747-76-0;3,5-dimethyl-N-phenyl-1H-pyrazole-4-carboxamide;SCHEMBL4631791;DTXSID30443744;TWQARRJUQHFBRS-UHFFFAOYSA-N;AKOS009606190;3,5-dimethyl-N-phenyl-4-pyrazolecarboxamide;N-Phenyl-3,5-dimethyl-1H-pyrazole-4-carboxamide

Suppliers and Price of 3,5-dimethyl-N-phenyl-1H-pyrazole-4-carboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-dimethyl-N-phenyl-1H-pyrazole-4-carboxamide

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:215.105862047
Heavy Atom Count:16
Complexity:251

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=NN1)C)C(=O)NC2=CC=CC=C2

Technology Process of 3,5-dimethyl-N-phenyl-1H-pyrazole-4-carboxamide

There total 5 articles about 3,5-dimethyl-N-phenyl-1H-pyrazole-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 102626-04-0
4-amino-3-phenyl-aminocarbonyl-3-penten-2-one

: 61747-76-0
3,5-dimethyl-4-phenylaminocarbonyl-1H-pyrazole

Guidance literature:: With hydrazine hydrochloride; In ethanol; for 1h; Heating;
DOI:10.1002/jhet.5570330441

Reference yield: 82.0%

: 260047-11-8
3,5-dimethyl-4-(N-phenylcarbamoyl)isoxazole

: 61747-76-0
3,5-dimethyl-4-phenylaminocarbonyl-1H-pyrazole

Guidance literature:: With hydrazine hydrate; nickel; In methanol; at 20 ℃;
DOI:10.1016/j.tet.2007.09.046

Reference yield:

: 2510-36-3
3,5-dimethyl-4-isoxazolecarboxylic acid

: 61747-76-0
3,5-dimethyl-4-phenylaminocarbonyl-1H-pyrazole

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride; DMF / CH₂Cl₂

2: triethylamine / CH₂Cl₂

3: 82 percent / hydrazine hydrate / Raney nickel / methanol / 20 °C

With oxalyl dichloride; hydrazine hydrate; triethylamine; N,N-dimethyl-formamide; nickel; In methanol; dichloromethane;
DOI:10.1016/j.tet.2007.09.046