CHEMBRDG-BB 4024859

Base Information

• Chemical Name: CHEMBRDG-BB 4024859
• CAS No.: 61806-76-6
• Molecular Formula: C12H19N
• Molecular Weight: 177.29
• Hs Code.: 2921499090
• Mol file: 61806-76-6.mol

Synonyms:N-benzylpentan-2-amine(SALTDATA: HCl);

Chemical Property of CHEMBRDG-BB 4024859

Chemical Property:

• Vapor Pressure: 0.028mmHg at 25°C
• Boiling Point: 245.778oC at 760 mmHg
• PKA: 9.97±0.19(Predicted)
• Flash Point: 95.767oC
• PSA: 12.03000
• Density: 0.898g/cm3
• LogP: 3.35570

Purity/Quality:

98%Min ^*data from raw suppliers

N-benzyl-2-pentanaminehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CHEMBRDG-BB 4024859

There total 8 articles about CHEMBRDG-BB 4024859 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-Pentanone (107-87-9) + benzylamine (100-46-9) → N-Benzyl-1-methylbutylamine (61806-76-6)

Guidance literature:

2-Pentanone; benzylamine; With formic acid; chlorido(8-quinolinolato-k²N,O)(η⁵-pentamethylcyclo-pentadienyl)rhodium(III); In ethyl acetate; at 0 - 40 ℃; Inert atmosphere; Cooling with ice; Schlenk tube;

With sodium hydrogencarbonate; In water; ethyl acetate; Product distribution / selectivity;

Reference yield: 88.0%

2-pentylamine (625-30-9) + benzyl alcohol (100-51-6,185532-71-2) → N-Benzyl-1-methylbutylamine (61806-76-6)

Guidance literature:

2-pentylamine; benzyl alcohol; With palladium on aluminium oxyhydroxide; In n-heptane; at 90 ℃; for 12h; Inert atmosphere;

With hydrogen; In n-heptane; at 25 ℃; for 6h; under 760.051 Torr;

DOI:10.1021/jo8026609

Reference yield: 48.0%

2-Pentanone (107-87-9) + Benzaldoxime (932-90-1) → N-Benzyl-1-methylbutylamine (61806-76-6)

Guidance literature:

With hydrogen; magnesium oxide; copper; at 220 ℃; under 11250.9 Torr;

DOI:10.1023/B:RUGC.0000030394.26179.a0

upstream raw materials:

2-Pentanone

benzylamine

Benzaldoxime

2-pentylamine

Downstream raw materials:

(R)‐2‐aminopentane

(S)-2-aminopentane

Refernces

• 1、 -. "NOVEL ORGANIC METAL COMPLEX AND PROCESS FOR PREPARING AMINE COMPOUND". Page/Page column 12. . Retrieved 2010/09/18.
• 2、 Burkhardt, Elizabeth R.,Coleridge, Brian M.. "Reductive amination with 5-ethyl-2-methylpyridine borane". . p. 5152 - 5155. Retrieved 2008/12/20.