Benzenamine, 3,6-dibromo-2,4-diiodo-

Base Information

Chemical Name:Benzenamine, 3,6-dibromo-2,4-diiodo-
CAS No.:618119-31-6
Molecular Formula:C6H3Br2I2N
Molecular Weight:502.714
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenamine, 3,6-dibromo-2,4-diiodo-

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Technology Process of Benzenamine, 3,6-dibromo-2,4-diiodo-

There total 1 articles about Benzenamine, 3,6-dibromo-2,4-diiodo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 3638-73-1
2,5-dibromoaniline

: 618119-31-6
3,6-dibromo-2,4-diiodoaniline

Guidance literature:: With sodium acetate; Iodine monochloride; In acetic acid; at 80 ℃; for 23h;
DOI:10.1021/jo0349227

Reference yield: 43.0%

: 618119-31-6
3,6-dibromo-2,4-diiodoaniline

: 618119-32-7
2,5-dibromo-1,3-diiodobenzene

Guidance literature:: With isopentyl nitrite; In N,N-dimethyl-formamide; at 65 - 70 ℃;
DOI:10.1021/jo0349227

Reference yield:

: 618119-31-6
3,6-dibromo-2,4-diiodoaniline

: 618119-40-7
2-[2,6-bis-(3,3-dimethyl-but-1-ynyl)-4-(3,5-di-pent-1-ynyl-benzyl)-phenyl]-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 7 steps

1.1: 43 percent / isoamylnitrite / dimethylformamide / 65 - 70 °C

2.1: 75 percent / CuI; Et₃N / (Ph₃P)2PdCl₂ / tetrahydrofuran / 24 h / 20 °C

3.1: t-BuLi / tetrahydrofuran / 0.5 h / -78 °C

3.2: 38 percent / tetrahydrofuran / -78 - 20 °C

4.1: 71 percent / p-TsOH / toluene / 1 h / Heating

5.1: n-BuLi / tetrahydrofuran / 0.5 h / -78 °C

5.2: 78 percent / tetrahydrofuran / -78 - 20 °C

6.1: NaH; imidazole / tetrahydrofuran / 0.5 h / 60 °C

6.2: tetrahydrofuran / 0.5 h / 60 °C

6.3: 83 percent / tetrahydrofuran / 0.5 h

7.1: 43 percent / AIBN; Bu₃SnH / toluene / 10 h / 80 °C

With 1H-imidazole; copper(l) iodide; n-butyllithium; 2,2'-azobis(isobutyronitrile); tert.-butyl lithium; tri-n-butyl-tin hydride; sodium hydride; toluene-4-sulfonic acid; triethylamine; isopentyl nitrite; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo0349227