Benzenepentanoyl chloride, 4-methoxy-

Base Information

Chemical Name:Benzenepentanoyl chloride, 4-methoxy-
CAS No.:61875-52-3
Molecular Formula:C12H15ClO2
Molecular Weight:226.703
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenepentanoyl chloride, 4-methoxy-

Chemical Property:

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Technology Process of Benzenepentanoyl chloride, 4-methoxy-

There total 6 articles about Benzenepentanoyl chloride, 4-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7508-04-5
5-(4-methoxyphenyl)pentanoic acid

: 61875-52-3
5-(4-methoxy-phenyl)-valeryl chloride

Guidance literature:: With thionyl chloride;
DOI:10.1080/00173130150503759

Reference yield:

: 15542-26-4,16913-48-7
(2E,4E)-ethyl 5-(4'-methoxyphenyl)penta-2,4-dienoate

: 61875-52-3
5-(4-methoxy-phenyl)-valeryl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 12 h

2: sodium hydroxide / ethanol / 12 h / 20 °C

3: oxalyl dichloride; N,N-dimethyl-formamide / tetrahydrofuran / 2 h / 20 °C

With oxalyl dichloride; palladium 10% on activated carbon; hydrogen; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; ethanol;
DOI:10.1016/j.bmc.2013.07.010

Reference yield:

: 79023-06-6
5-(4-methoxyphenyl)pentanoic acid ethyl ester

: 61875-52-3
5-(4-methoxy-phenyl)-valeryl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / ethanol / 12 h / 20 °C

2: oxalyl dichloride; N,N-dimethyl-formamide / tetrahydrofuran / 2 h / 20 °C

With oxalyl dichloride; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; ethanol;
DOI:10.1016/j.bmc.2013.07.010