Cyanamide, [(4-chlorophenyl)methyl]-

Base Information

• Chemical Name: Cyanamide, [(4-chlorophenyl)methyl]-
• CAS No.: 61883-69-0
• Molecular Formula: C8H7ClN2
• Molecular Weight: 166.60800
• Mol file: 61883-69-0.mol

Synonyms:4-Chlor-benzylcyanamid;4-Chloro-benzyl-cyanamide;

Chemical Property of Cyanamide, [(4-chlorophenyl)methyl]-

Chemical Property:

• Melting Point: 91 - 92 °C (diethyl ether)
• PSA: 35.82000
• LogP: 2.30158

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Cyanamide, [(4-chlorophenyl)methyl]-

There total 2 articles about Cyanamide, [(4-chlorophenyl)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bromocyane (506-68-3) + 4-chlorobenzylamine (104-86-9) → (4-chloro-benzyl)-cyanamide (61883-69-0)

Guidance literature:

With sodium carbonate; In tetrahydrofuran; at -20 - 0 ℃;

DOI:10.1055/s-1976-24127

Reference yield:

→ (4-chloro-benzyl)-cyanamide (61883-69-0)

Guidance literature:

4-Chlor-benzylamin in Ae., Bromcyan in Ae., 20grad, 75 min;

DOI:10.1139/v61-130

Reference yield:

(4-chloro-benzyl)-cyanamide (61883-69-0) → N-(4-chloro)benzyl-N'-hydroxyguanidine

Guidance literature:

With hydroxylamine hydrochloride; potassium carbonate; In ethanol; at 20 ℃; for 5h;

DOI:10.1016/S0968-0896(02)00155-4

upstream raw materials:

bromocyane

4-chlorobenzylamine

Downstream raw materials:

(4-chloro-benzyl)-(4-methyl-oxazol-2-yl)-amine

Refernces

• 1、 Cai, Tingwei,Xian, Ming,Wang, Peng George. "Electrochemical and peroxidase oxidation study of N'-hydroxyguanidine derivatives as NO donors.". . p. 1507 - 1510. Retrieved 2007/10/03.