[2-(Methoxymethyl)-6-nitrophenyl]methanol

Base Information

Chemical Name:[2-(Methoxymethyl)-6-nitrophenyl]methanol
CAS No.:61940-25-8
Molecular Formula:C9H11NO4
Molecular Weight:197.191
Hs Code.:
DSSTox Substance ID:DTXSID80708133
Wikidata:Q82642246

Synonyms:[2-(Methoxymethyl)-6-nitrophenyl]methanol;61940-25-8;SCHEMBL11863227;DTXSID80708133

Suppliers and Price of [2-(Methoxymethyl)-6-nitrophenyl]methanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [2-(Methoxymethyl)-6-nitrophenyl]methanol

Chemical Property:

XLogP3:0.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:197.06880783
Heavy Atom Count:14
Complexity:192

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COCC1=C(C(=CC=C1)[N+](=O)[O-])CO

Technology Process of [2-(Methoxymethyl)-6-nitrophenyl]methanol

There total 5 articles about [2-(Methoxymethyl)-6-nitrophenyl]methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 61940-24-7
2-(α-methoxymethyl)-6-nitrobenzoic acid

: 61940-25-8
[2-(methoxymethyl)-6-nitro-phenyl]methanol

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water;

Reference yield: 80.0%

: 61940-23-6
methyl 2-(methoxymethyl)-6-nitro-benzoate

: 61940-25-8
[2-(methoxymethyl)-6-nitro-phenyl]methanol

Guidance literature:: With methanol; lithium borohydride; In tetrahydrofuran; at 0 - 20 ℃; for 3h; Inert atmosphere;

Reference yield:

: 42760-46-3
7-nitro-3H-isobenzofuran-1-one

: 61940-25-8
[2-(methoxymethyl)-6-nitro-phenyl]methanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / tetrahydrofuran / 0.75 h / 50 °C

2.1: sodium hydride / N,N-dimethyl acetamide; mineral oil / 0.5 h / 0 - 20 °C / Inert atmosphere

2.2: 0 - 20 °C

3.1: lithium borohydride; methanol / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

With methanol; lithium borohydride; sodium hydride; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl acetamide; mineral oil;