N-(4,5-dichloro-2-nitrophenyl)-4-nitrobenzenesulfonamide

Base Information

• Chemical Name: N-(4,5-dichloro-2-nitrophenyl)-4-nitrobenzenesulfonamide
• CAS No.: 15312-13-7
• Molecular Formula: C₁₂H₇Cl₂N₃O₆S
• Molecular Weight: 392.176
• Mol file: 15312-13-7.mol

Synonyms:Benzenesulfonamide,N-(3,4-dichloro-2-nitrophenyl)-4-nitro- (9CI); Benzenesulfonanilide, 3',4'-dichloro-2',4-dinitro-(8CI); 1,2-Dichloro-4-(p-nitrobenzenesulfonylamido)-5-nitrobenzene; NSC 400957

Chemical Property of N-(4,5-dichloro-2-nitrophenyl)-4-nitrobenzenesulfonamide

Chemical Property:

• Vapor Pressure: 2.33E-12mmHg at 25°C
• Boiling Point: 555°Cat760mmHg
• Flash Point: 289.5°C
• Density: 1.734g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(4,5-dichloro-2-nitrophenyl)-4-nitrobenzenesulfonamide

There total 3 articles about N-(4,5-dichloro-2-nitrophenyl)-4-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(3,4-dichlorophenyl)-4-nitrobenzenesulfonamide (330221-06-2) → 4-nitro-benzenesulfonic acid-(4,5-dichloro-2-nitro-anilide) (15312-13-7)

Guidance literature:

With nitric acid;

DOI:10.1021/ja01141a068

Reference yield:

m,p-dichloroaniline (95-76-1) → 4-nitro-benzenesulfonic acid-(4,5-dichloro-2-nitro-anilide) (15312-13-7)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH solution

2: HNO₃

With sodium hydroxide; nitric acid;

DOI:10.1021/ja01141a068

Reference yield:

4-Nitrobenzenesulfonyl chloride (98-74-8) → 4-nitro-benzenesulfonic acid-(4,5-dichloro-2-nitro-anilide) (15312-13-7)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH solution

2: HNO₃

With sodium hydroxide; nitric acid;

DOI:10.1021/ja01141a068

upstream raw materials:

N-(3,4-dichlorophenyl)-4-nitrobenzenesulfonamide

m,p-dichloroaniline

4-Nitrobenzenesulfonyl chloride

Downstream raw materials:

sulfanilic acid-(2-amino-4,5-dichloro-anilide)