perchloric acid;6-phenyl-2,3-dihydro-1H-1,4-diazepine

Base Information

Chemical Name:perchloric acid;6-phenyl-2,3-dihydro-1H-1,4-diazepine
CAS No.:62084-97-3
Molecular Formula:C₁₁H₁₂N₂*ClHO₄
Molecular Weight:272.688
Hs Code.:
DSSTox Substance ID:DTXSID20499210

Synonyms:62084-97-3;DTXSID20499210;Perchloric acid--6-phenyl-2,3-dihydro-1H-1,4-diazepine (1/1)

Suppliers and Price of perchloric acid;6-phenyl-2,3-dihydro-1H-1,4-diazepine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of perchloric acid;6-phenyl-2,3-dihydro-1H-1,4-diazepine

Chemical Property:

Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:1
Exact Mass:272.0563846
Heavy Atom Count:18
Complexity:326

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CN=CC(=CN1)C2=CC=CC=C2.OCl(=O)(=O)=O

Technology Process of perchloric acid;6-phenyl-2,3-dihydro-1H-1,4-diazepine

There total 3 articles about perchloric acid;6-phenyl-2,3-dihydro-1H-1,4-diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 7089-34-1
((Z)-3-Dimethylamino-2-phenyl-allylidene)-dimethyl-ammonium; perchlorate

: 107-15-3,85404-18-8
ethylenediamine

: 62084-97-3
2,3-dihydro-6-phenyl-1,4-diazepinium perchlorate

Guidance literature:: In methanol; for 0.333333h; Heating;
DOI:10.1039/P19810000726

Reference yield: 76.0%

: 7089-34-1
((E)-3-Dimethylamino-2-phenyl-allylidene)-dimethyl-ammonium; perchlorate

: 107-15-3,85404-18-8
ethylenediamine

: 62084-97-3
2,3-dihydro-6-phenyl-1,4-diazepinium perchlorate

Guidance literature:: With perchloric acid; In methanol; 1.) 60 deg C; 2.) 24 h, room temp;

Reference yield:

: 103-82-2
phenylacetic acid

: 62084-97-3
2,3-dihydro-6-phenyl-1,4-diazepinium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / POCl₃ / 80 - 90 °C

2: 89 percent / methanol / 0.33 h / Heating

With trichlorophosphate; In methanol;
DOI:10.1039/P19810000726