2-Butenoic acid, 3-(2-methoxy-4-methylphenyl)-, (Z)-

Base Information

Chemical Name:2-Butenoic acid, 3-(2-methoxy-4-methylphenyl)-, (Z)-
CAS No.:62155-72-0
Molecular Formula:C12H14O3
Molecular Weight:206.241
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Butenoic acid, 3-(2-methoxy-4-methylphenyl)-, (Z)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 2-Butenoic acid, 3-(2-methoxy-4-methylphenyl)-, (Z)-

There total 5 articles about 2-Butenoic acid, 3-(2-methoxy-4-methylphenyl)-, (Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: Ethyl (2Z)-3-(2-methoxy-4-methylphenyl)but-2-enoate

: 62155-72-0
(Z)-3-(2-methoxy-4-methylphenyl)but-2-enoic acid

Guidance literature:: With sodium hydroxide; In methanol; water; at 20 ℃; for 12h;
DOI:10.1016/j.tetlet.2016.12.017

Reference yield:

: 35633-35-3
2-methoxy-4-methylacetophenone

: 62155-72-0
(Z)-3-(2-methoxy-4-methylphenyl)but-2-enoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran / Reflux

2: sodium hydroxide / water; methanol / 12 h / 20 °C

With sodium hydride; sodium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.tetlet.2016.12.017

Reference yield:

: 6921-64-8
4'-hydroxy-2'-methylacetophenone

: 62155-72-0
(Z)-3-(2-methoxy-4-methylphenyl)but-2-enoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide

2: sodium hydride / tetrahydrofuran / Reflux

3: sodium hydroxide / water; methanol / 12 h / 20 °C

With sodium hydride; potassium hydroxide; sodium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.tetlet.2016.12.017