1,2-Bis(4-methoxyphenyl)hydrazine

Base Information

• Chemical Name: 1,2-Bis(4-methoxyphenyl)hydrazine
• CAS No.: 1027-40-3
• Molecular Formula: C14H16 N2 O2
• Molecular Weight: 244.293
• NSC Number: 86489
• DSSTox Substance ID: DTXSID30292931
• Nikkaji Number: J760.258H
• Wikidata: Q82031442
• Mol file: 1027-40-3.mol

Synonyms:1,2-bis(4-methoxyphenyl)hydrazine;1027-40-3;Hydrazine, 1,2-bis(4-methoxyphenyl)-;NSC86489;SCHEMBL851498;DTXSID30292931;NSC-86489

Chemical Property of 1,2-Bis(4-methoxyphenyl)hydrazine

Chemical Property:

• Vapor Pressure: 0.000479mmHg at 25°C
• Boiling Point: 314°Cat760mmHg
• Flash Point: 132.5°C
• Density: 1.196g/cm³
• XLogP3: 3.7
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 244.121177757
• Heavy Atom Count: 18
• Complexity: 198

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)NNC2=CC=C(C=C2)OC

Technology Process of 1,2-Bis(4-methoxyphenyl)hydrazine

There total 8 articles about 1,2-Bis(4-methoxyphenyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

(E)-1,2-bis(4-methoxyphenyl)diazene (501-58-6,21650-55-5,82570-64-7) → bis(4-methoxyphenyl)hydrazine (1027-40-3)

Guidance literature:

With sodium dithionite; 1,1′-dioctyl-4,4′-bipyridinium; potassium carbonate; In water; acetonitrile; at 35 ℃; for 1h;

DOI:10.1016/S0040-4039(96)01451-7

Reference yield: 91.0%

4,4'-azoxy anisole (1562-94-3,21650-70-4,51437-65-1) → bis(4-methoxyphenyl)hydrazine (1027-40-3)

Guidance literature:

With sodium dithionite; 1,1′-dioctyl-4,4′-bipyridinium; potassium carbonate; In water; acetonitrile; at 35 ℃; for 2h;

DOI:10.1016/S0040-4039(96)01451-7

Reference yield:

4-methoxy-aniline (104-94-9) → bis(4-methoxyphenyl)hydrazine (1027-40-3)

Guidance literature:

4-methoxy-aniline; With manganese(IV) oxide; In toluene; for 10h; Reflux;

With ammonium chloride; zinc; In water; acetone; at 20 ℃; for 5h;

DOI:10.1039/c9gc00515c

upstream raw materials:

para-methoxynitrobenzene

4,4'-azoxy anisole

(E)-1,2-bis(4-methoxyphenyl)diazene

4-methoxy-aniline

Downstream raw materials:

bis(4-methoxyphenyl)diazene