Technology Process of Benzenamine, 4-[(4-butoxyphenyl)thio]-
There total 6 articles about Benzenamine, 4-[(4-butoxyphenyl)thio]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: nickel (II) chloride hexahydrate; tetrabutylammomium bromide; potassium hydroxide / 12 h / 110 °C / Inert atmosphere
2: hydrogen bromide / 4 h / Inert atmosphere; Reflux
3: potassium carbonate; potassium iodide / acetonitrile / Inert atmosphere; Reflux
4: tin(II)chloride dihydrate; ethanol / 1 h / 70 °C / Inert atmosphere
With
tin(II)chloride dihydrate; nickel (II) chloride hexahydrate; ethanol; tetrabutylammomium bromide; hydrogen bromide; potassium carbonate; potassium iodide; potassium hydroxide;
In
acetonitrile;
DOI:10.2174/157018012799859909
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogen bromide / 4 h / Inert atmosphere; Reflux
2: potassium carbonate; potassium iodide / acetonitrile / Inert atmosphere; Reflux
3: tin(II)chloride dihydrate; ethanol / 1 h / 70 °C / Inert atmosphere
With
tin(II)chloride dihydrate; ethanol; hydrogen bromide; potassium carbonate; potassium iodide;
In
acetonitrile;
DOI:10.2174/157018012799859909