1,3-Dibromo-2-tert-butylsulfanylbenzene

Base Information

Chemical Name:1,3-Dibromo-2-tert-butylsulfanylbenzene
CAS No.:62261-15-8
Molecular Formula:C10H12Br2S
Molecular Weight:324.079
Hs Code.:
DSSTox Substance ID:DTXSID30352049
Wikidata:Q82128995

Synonyms:1,3-dibromo-2-tert-butylsulfanylbenzene;2-(tert-butylthio)-1,3-dibromobenzene;62261-15-8;ST026238;DTXSID30352049;t-butyl 2,6-dibromophenyl sulfide;AKOS000664185

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Dibromo-2-tert-butylsulfanylbenzene

Chemical Property:

XLogP3:4.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:323.90060
Heavy Atom Count:13
Complexity:155

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)SC1=C(C=CC=C1Br)Br

Technology Process of 1,3-Dibromo-2-tert-butylsulfanylbenzene

There total 2 articles about 1,3-Dibromo-2-tert-butylsulfanylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 62261-14-7
2,6-dibromobenzenethiol

: 75-65-0
tert-butyl alcohol

: 62261-15-8
2,6-dibromo-1-(tert-butylthio)benzene

Guidance literature:: 2,6-dibromobenzenethiol; tert-butyl alcohol; With acetic anhydride; acetic acid; at 0 ℃; for 0.333333h; Inert atmosphere; Schlenk technique;

With perchloric acid; In water; at 0 - 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.poly.2014.06.050

Reference yield:

: 608-30-0
2,6-dibromoaniline

: 62261-15-8
2,6-dibromo-1-(tert-butylthio)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: (i) aq. HCl, NaNO₂, (ii) aq. (EtOCS₂)2Ca

2: aq. H₂SO₄

With sulfuric acid;
DOI:10.1007/BF00973397

Reference yield: 69.0%

: 62261-15-8
2,6-dibromo-1-(tert-butylthio)benzene

: 5720-06-9
2-Methoxyphenylboronic acid

: (3-bromo-2'-methoxy-[1,1'-biphenyl]-2-yl)(tert-butyl)sulfane

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; lithium chloride; In 1,4-dioxane; water; for 24h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2016.03.040