2-Butenal, 2-methyl-4-phenoxy-, (E)-

Base Information

Chemical Name:2-Butenal, 2-methyl-4-phenoxy-, (E)-
CAS No.:62285-79-4
Molecular Formula:C11H12O2
Molecular Weight:176.215
Hs Code.:

Synonyms:

Suppliers and Price of 2-Butenal, 2-methyl-4-phenoxy-, (E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-Butenal, 2-methyl-4-phenoxy-, (E)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Butenal, 2-methyl-4-phenoxy-, (E)-

There total 8 articles about 2-Butenal, 2-methyl-4-phenoxy-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 99321-86-5
(E)-2-methyl-4-phenoxybut-2-en-1-ol

: 62285-79-4
(E)-2-methyl-4-phenoxybut-2-enal

Guidance literature:: With sulfur trioxide pyridine complex; triethylamine; In dimethyl sulfoxide; at 0 - 20 ℃; for 0.5h;
DOI:10.1039/c9ob02339a

Reference yield:

: 14309-15-0
phenyl prenyl ether

: 62285-79-4
(E)-2-methyl-4-phenoxybut-2-enal

Guidance literature:: Multi-step reaction with 5 steps

1: Ca(OCl)2, dry ice / CH₂Cl₂; H₂O / 10 °C

2: ethanol; H₂O / Ambient temperature

3: 40 percent peracetic acid, Na₂CO₃ / CH₂Cl₂ / 0.5 h

4: ethyl acetate / 0.5 h / 40 - 50 °C

5: MeI / CHCl₃ / 3 h / Heating

With peracetic acid; calcium hypochlorite; Methamphetamin; sodium carbonate; methyl iodide; In ethanol; dichloromethane; chloroform; water; ethyl acetate;
DOI:10.1246/cl.1986.2035

Reference yield:

: 108-95-2,27073-41-2
phenol

: 62285-79-4
(E)-2-methyl-4-phenoxybut-2-enal

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 12 h / 0 - 20 °C

2: tert.-butylhydroperoxide; selenium(IV) oxide / dichloromethane; water / 48 h / 0 - 20 °C

3: triethylamine; sulfur trioxide pyridine complex / dimethyl sulfoxide / 0.5 h / 0 - 20 °C

With tert.-butylhydroperoxide; selenium(IV) oxide; sulfur trioxide pyridine complex; potassium carbonate; triethylamine; In dichloromethane; water; dimethyl sulfoxide; acetonitrile; 1: |Williamson Ether Synthesis / 3: |Parikh-Doering Oxidation;
DOI:10.1039/c9ob02339a