Glycine, N-[(2-hydroxyphenyl)methylene]-

Base Information

• Chemical Name: Glycine, N-[(2-hydroxyphenyl)methylene]-
• CAS No.: 6343-78-8
• Molecular Formula: C9H9 N O3
• Molecular Weight: 179.175
• NSC Number: 49747
• DSSTox Substance ID: DTXSID90419788
• Nikkaji Number: J1.013.232K,J3.078.399I

Synonyms:6343-78-8;Glycine, N-[(2-hydroxyphenyl)methylene]-;salicylideneglycine;NSC49747;N-salicyl-idenglycine;Enamine_005977;Oprea1_780649;SCHEMBL3391389;SCHEMBL3391391;SCHEMBL12892300;DTXSID90419788;NSC-49747;AKOS027461412;IDI1_008212;[(2-Hydroxyphenyl)methylidene amino]acetic acid;2-[(E)-(2-hydroxyphenyl)methyleneamino]acetic acid

Chemical Property of Glycine, N-[(2-hydroxyphenyl)methylene]-

Chemical Property:

• Vapor Pressure: 1.07E-07mmHg at 25°C
• Boiling Point: 405.2°Cat760mmHg
• Flash Point: 198.8°C
• Density: 1.414g/cm³
• XLogP3: 1.1
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 179.058243149
• Heavy Atom Count: 13
• Complexity: 203

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C(=C1)C=NCC(=O)O)O

Technology Process of Glycine, N-[(2-hydroxyphenyl)methylene]-

There total 5 articles about Glycine, N-[(2-hydroxyphenyl)methylene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

salicylaldehyde (90-02-8) + glycine (56-40-6,18875-39-3,25718-94-9) → N-salicylideneglycine (6343-78-8)

Guidance literature:

With potassium hydroxide; In methanol; for 0.0833333h;

Reference yield:

salicylaldehyde (90-02-8) + glycine (56-40-6,18875-39-3,25718-94-9) → N-(o-hydroxybenzylidene)glycine (6343-78-8)

Guidance literature:

With sodium hydroxide; In water;

DOI:10.1016/S0040-4020(01)91449-8

Reference yield:

copper(II) bis(salicylaldehyde) + glycine (56-40-6,18875-39-3,25718-94-9) → N-salicylideneglycine (6343-78-8)

Guidance literature:

In ethanol;

DOI:10.1246/bcsj.40.2826

upstream raw materials:

salicylaldehyde

glycine

UO₂(N-salicylidineglycine)(H₂O)

2-methyl-benzyl alcohol

Downstream raw materials:

salicylaldehyde

glycine

Re(C₆H₄OCHNCH₂COO)Cl(P(C₆H₅)3)2

[2-(2-hydroxybenzylideneamino)acetato](imidazole)copper(II)

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