Benzamide, 2-(2-hydroxyethyl)-N-[2-(3-methoxyphenyl)ethyl]-

Base Information

Chemical Name:Benzamide, 2-(2-hydroxyethyl)-N-[2-(3-methoxyphenyl)ethyl]-
CAS No.:62310-88-7
Molecular Formula:C18H21NO3
Molecular Weight:299.37
Hs Code.:
DSSTox Substance ID:DTXSID40486460
Wikidata:Q82327427

Synonyms:62310-88-7;Benzamide, 2-(2-hydroxyethyl)-N-[2-(3-methoxyphenyl)ethyl]-;DTXSID40486460

Suppliers and Price of Benzamide, 2-(2-hydroxyethyl)-N-[2-(3-methoxyphenyl)ethyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzamide, 2-(2-hydroxyethyl)-N-[2-(3-methoxyphenyl)ethyl]-

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:299.15214353
Heavy Atom Count:22
Complexity:334

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC(=C1)CCNC(=O)C2=CC=CC=C2CCO

Technology Process of Benzamide, 2-(2-hydroxyethyl)-N-[2-(3-methoxyphenyl)ethyl]-

There total 2 articles about Benzamide, 2-(2-hydroxyethyl)-N-[2-(3-methoxyphenyl)ethyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 4702-34-5
isochroman-1-one

: 2039-67-0
2-(3-methoxyphenyl)-1-ethanamine

: 62310-88-7
2-(2-hydroxyethyl)-N-[2-(3-methoxyphenyl)ethyl]benzamide

Guidance literature:: With potassium cyanide; at 75 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tetlet.2017.08.007

Reference yield:

: 62310-88-7
2-(2-hydroxyethyl)-N-[2-(3-methoxyphenyl)ethyl]benzamide

Guidance literature:: /BRN= 775202/, /BRN= 124656/;
DOI:10.1055/s-1976-24169

Reference yield:

: 62310-88-7
2-(2-hydroxyethyl)-N-[2-(3-methoxyphenyl)ethyl]benzamide

: 7-methyl-5,6,7,8,9,14-hexahydrodibenzo[d,g]azecin-3-yl benzoate

Guidance literature:: Multi-step reaction with 5 steps

1: trichlorophosphate / acetonitrile / 0 - 24 °C / Reflux; Inert atmosphere

2: acetonitrile / Inert atmosphere

3: boron tribromide / chloroform / 24 h / 0 - 20 °C / Inert atmosphere; Cooling with ice

4: sodium; ammonia / -78 - 20 °C / Inert atmosphere

5: sodium hydride / dichloromethane / 0 - 20 °C / Inert atmosphere

With ammonia; sodium; boron tribromide; sodium hydride; trichlorophosphate; In dichloromethane; chloroform; acetonitrile;
DOI:10.1016/j.tetlet.2017.08.007