4-Bromo-1-methoxy-2-(methoxymethoxy)benzene

Base Information

Chemical Name:4-Bromo-1-methoxy-2-(methoxymethoxy)benzene
CAS No.:623550-16-3
Molecular Formula:C9H11BrO3
Molecular Weight:247.089
Hs Code.:
DSSTox Substance ID:DTXSID80471411
Wikidata:Q82299913

Synonyms:4-bromo-1-methoxy-2-(methoxymethoxy)benzene;623550-16-3;4-Bromo-1-methoxy-2-methoxymethoxy-benzene;Benzene, 4-bromo-1-methoxy-2-(methoxymethoxy)-;SCHEMBL2178750;DTXSID80471411;TWHPNWMJJYXOSY-UHFFFAOYSA-N;MFCD27926525;4-Bromo-1-methoxy-2-methoxymethoxybenzene;CS-0193547;E93164;A1-05127

Suppliers and Price of 4-Bromo-1-methoxy-2-(methoxymethoxy)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

A1 Biochem Labs
4-Bromo-1-methoxy-2-methoxymethoxy-benzene 95%
5 g
$ 600.00

AOBChem
4-Bromo-1-methoxy-2-(methoxymethoxy)benzene 95%
500mg
$ 128.00

Chemcia Scientific
4-Bromo-1-methoxy-2-methoxymethoxy-benzene ＞95%
5 G
$ 615.00

Matrix Scientific
4-Bromo-1-methoxy-2-methoxymethoxy-benzene
5g
$ 990.00

Total 1 raw suppliers

Chemical Property of 4-Bromo-1-methoxy-2-(methoxymethoxy)benzene

Chemical Property:

PSA：27.69000
LogP:2.44040
XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:245.98916
Heavy Atom Count:13
Complexity:143

Purity/Quality:: 4-Bromo-1-methoxy-2-methoxymethoxy-benzene 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COCOC1=C(C=CC(=C1)Br)OC

Technology Process of 4-Bromo-1-methoxy-2-(methoxymethoxy)benzene

There total 4 articles about 4-Bromo-1-methoxy-2-(methoxymethoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 37942-01-1
5-bromo-2-methoxyphenol

: 107-30-2
chloromethyl methyl ether

: 623550-16-3
4-bromo-1-methoxy-2-(methoxymethoxy)benzene

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 8.5h; Inert atmosphere;
DOI:10.1021/acs.orglett.9b04337

Reference yield:

: 531-37-3
2-methoxyphenyl benzoate

: 623550-16-3
4-bromo-1-methoxy-2-(methoxymethoxy)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: Br₂; AcOH / 20 °C

2: K₂CO₃ / methanol / 20 °C

3: 88 percent / iPr₂NEt / CH₂Cl₂ / 4 h / 0 - 20 °C

With bromine; potassium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;
DOI:10.1021/ol035443x

Reference yield:

: 159783-14-9
5-bromo-2-methoxyphenyl benzoate

: 623550-16-3
4-bromo-1-methoxy-2-(methoxymethoxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / methanol / 20 °C

2: 88 percent / iPr₂NEt / CH₂Cl₂ / 4 h / 0 - 20 °C

With potassium carbonate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;
DOI:10.1021/ol035443x